2-Octenoic acid, 5-[(phenylmethyl)amino]-, ethyl ester, (2E)-

Base Information

Chemical Name:2-Octenoic acid, 5-[(phenylmethyl)amino]-, ethyl ester, (2E)-
CAS No.:482358-59-8
Molecular Formula:C17H25NO2
Molecular Weight:275.391
Hs Code.:

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Chemical Property of 2-Octenoic acid, 5-[(phenylmethyl)amino]-, ethyl ester, (2E)-

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Technology Process of 2-Octenoic acid, 5-[(phenylmethyl)amino]-, ethyl ester, (2E)-

There total 3 articles about 2-Octenoic acid, 5-[(phenylmethyl)amino]-, ethyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 561014-38-8
ethyl (E)-5-(N-allyl-N-benzylamino)oct-2-enoate

: 482358-59-8
ethyl (E)-5-(N-benzylamino)oct-2-enoate

Guidance literature:: With 1,3-dimethylbarbituric acid; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1081/SCC-120016308

Reference yield:

: 4383-22-6
Allylbenzylamine

: 482358-59-8
ethyl (E)-5-(N-benzylamino)oct-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: molecular sieves 4 Angstroem / tetrahydrofuran

2.1: Zn; TMSCl / diethyl ether; tetrahydrofuran / 0.08 h / Heating

2.2: diethyl ether; tetrahydrofuran / 8 h / 35 °C

3.1: 75 percent / N,N-dimethylbarbituric acid / CH₂Cl₂ / 24 h / 20 °C

With chloro-trimethyl-silane; 1,3-dimethylbarbituric acid; 4 A molecular sieve; zinc; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1081/SCC-120016308

Reference yield:

: 100-39-0
benzyl bromide

: 482358-59-8
ethyl (E)-5-(N-benzylamino)oct-2-enoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 74 percent / K₂CO₃ / 11 h / 20 °C

2.1: molecular sieves 4 Angstroem / tetrahydrofuran

3.1: Zn; TMSCl / diethyl ether; tetrahydrofuran / 0.08 h / Heating

3.2: diethyl ether; tetrahydrofuran / 8 h / 35 °C

4.1: 75 percent / N,N-dimethylbarbituric acid / CH₂Cl₂ / 24 h / 20 °C

With chloro-trimethyl-silane; 1,3-dimethylbarbituric acid; 4 A molecular sieve; potassium carbonate; zinc; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1081/SCC-120016308