14-Methyl-15-oxocholest-7-en-3-yl benzoate

Base Information

Chemical Name:14-Methyl-15-oxocholest-7-en-3-yl benzoate
CAS No.:26313-82-6
Molecular Formula:C₃₅H₅₀O₃
Molecular Weight:518.78
Hs Code.:
NSC Number:106561
DSSTox Substance ID:DTXSID30949170

Synonyms:26313-82-6;14-methyl-15-oxocholest-7-en-3-yl benzoate;NSC106561;DTXSID30949170;NSC-106561;A25426

Suppliers and Price of 14-Methyl-15-oxocholest-7-en-3-yl benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 14-Methyl-15-oxocholest-7-en-3-yl benzoate

Chemical Property:

Vapor Pressure:4.8E-14mmHg at 25°C
Boiling Point:593.3°Cat760mmHg
Flash Point:244.8°C
Density:1.07g/cm³
XLogP3:9.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:8
Exact Mass:518.37599545
Heavy Atom Count:38
Complexity:928

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)CCCC(C)C1CC(=O)C2(C1(CCC3C2=CCC4C3(CCC(C4)OC(=O)C5=CC=CC=C5)C)C)C

Technology Process of 14-Methyl-15-oxocholest-7-en-3-yl benzoate

There total 5 articles about 14-Methyl-15-oxocholest-7-en-3-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7654-37-7
(3β,5α)-3-(benzoyloxy)cholest-8(14)-en-15-one

: 74-88-4
methyl iodide

: 64768-25-8
3β-methoxy-14-methyl-5α-cholest-7-en-15-one

: 26313-82-6
(3β,5α,14α)-3-(benzoyloxy)-14-methylcholest-7-en-15-one

: 64768-24-7
(3β,5α,14α)-3-hydroxy-14-methylcholest-7-en-15-one

Guidance literature:: With potassium tert-butylate; Yield given. Multistep reaction. Yields of byproduct given; 1.) t-BuOK, THF, 10 min, 2.) t-BuOH, THF, 2 h;
DOI:10.1021/jo00371a025

Reference yield:

: 34227-12-8
(3β,5α)-cholesta-7,14-dien-3-ol benzoate

: 26313-82-6
(3β,5α,14α)-3-(benzoyloxy)-14-methylcholest-7-en-15-one

Guidance literature:: Multi-step reaction with 2 steps

1: monoperoxyphthalic acid / Behandeln des Reaktionsprodukts mit aethanol. HCl

2: potassium tert-butylate

With monoperoxyphthalic acid; potassium tert-butylate;