Technology Process of Stannane, triethyl(phenylmethyl)-
There total 15 articles about Stannane, triethyl(phenylmethyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Zn; NH4Cl;
In
tetrahydrofuran; water;
air; addn. of organotin (1 equiv.) to suspension of Zn-powder (2 equivs.) in satd. soln. of NH4Cl in H2O:THF, dropwise addn. of benzyl bromide (2 equivs.) with rate maintaining gentle reflux, stirring with cooling toroom temp. for 30 min; sepn. of org. layer, evapn., distillation (vac.); elem. anal.;
DOI:10.1021/om9507742
- Guidance literature:
-
Multi-step reaction with 5 steps
1: benzene
2: CH3OH / methanol
With
CH3OH;
In
methanol; benzene;
- Guidance literature:
-
Multi-step reaction with 7 steps
3: benzene
4: CH3OH / methanol
5: n-heptane
6: n-heptane
With
CH3OH;
In
methanol; n-heptane; benzene;