Propanoic acid, 2,2-dimethyl-, 2-(azidomethyl)-4-(3,4-dimethylphenyl)butyl ester

Base Information

Chemical Name:Propanoic acid, 2,2-dimethyl-, 2-(azidomethyl)-4-(3,4-dimethylphenyl)butyl ester
CAS No.:503597-11-3
Molecular Formula:C₁₈H₂₇N₃O₂
Molecular Weight:317.431
Hs Code.:

Synonyms:

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Chemical Property of Propanoic acid, 2,2-dimethyl-, 2-(azidomethyl)-4-(3,4-dimethylphenyl)butyl ester

Chemical Property:

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Technology Process of Propanoic acid, 2,2-dimethyl-, 2-(azidomethyl)-4-(3,4-dimethylphenyl)butyl ester

There total 7 articles about Propanoic acid, 2,2-dimethyl-, 2-(azidomethyl)-4-(3,4-dimethylphenyl)butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 503597-07-7
2-(3,4-dimethylphenethyl)-1,3-propanediol

: 503597-11-3
2-(azidomethyl)-4-(3,4-dimethylphenyl)butyl pivalate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

2: 82 percent / PPh₃; diethyl azodicarboxylate; diphenylphosphoryl azide / tetrahydrofuran / 18 h / 20 °C

With pyridine; diphenylphosphoranyl azide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2003.12.005

Reference yield:

: 503597-05-5
diethyl 2-(3,4-dimethylphenethyl)malonate

: 503597-11-3
2-(azidomethyl)-4-(3,4-dimethylphenyl)butyl pivalate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / LiAlH₄ / diethyl ether / 3 h / 20 °C

2: 84 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

3: 82 percent / PPh₃; diethyl azodicarboxylate; diphenylphosphoryl azide / tetrahydrofuran / 18 h / 20 °C

With pyridine; lithium aluminium tetrahydride; diphenylphosphoranyl azide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.bmc.2003.12.005

Reference yield:

: 3020-06-2
3,4-dimethylphenylacetonitrile

: 503597-11-3
2-(azidomethyl)-4-(3,4-dimethylphenyl)butyl pivalate

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / H₂SO₄ / 72 h / Heating

2: 60 percent / LiAlH₄ / diethyl ether / 0.5 h / 20 °C

3: 91 percent / PPh₃; CBr₄ / tetrahydrofuran / 3 h / 20 °C

4: 76 percent / NaH / dimethylformamide / 16 h / 20 °C

5: 74 percent / LiAlH₄ / diethyl ether / 3 h / 20 °C

6: 84 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

7: 82 percent / PPh₃; diethyl azodicarboxylate; diphenylphosphoryl azide / tetrahydrofuran / 18 h / 20 °C

With pyridine; lithium aluminium tetrahydride; carbon tetrabromide; sulfuric acid; diphenylphosphoranyl azide; sodium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2003.12.005