N-[4-(3,4-dimethylphenyl)-2-(pivaloyloxymethyl)butyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

Base Information

Chemical Name:N-[4-(3,4-dimethylphenyl)-2-(pivaloyloxymethyl)butyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea
CAS No.:503597-14-6
Molecular Formula:C₂₉H₄₂N₂O₅S
Molecular Weight:530.729
Hs Code.:

Synonyms:N-[4-(3,4-dimethylphenyl)-2-(pivaloyloxymethyl)butyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

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Chemical Property of N-[4-(3,4-dimethylphenyl)-2-(pivaloyloxymethyl)butyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

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Technology Process of N-[4-(3,4-dimethylphenyl)-2-(pivaloyloxymethyl)butyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

There total 10 articles about N-[4-(3,4-dimethylphenyl)-2-(pivaloyloxymethyl)butyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 503598-02-5
2,2-dimethyl-propionic acid 2-aminomethyl-4-(3,4-dimethyl-phenyl)-butyl ester

: 289903-62-4
4-[(methoxylmethyl)oxy]-3-methoxybenzyl isothiocyanate

: 503597-14-6
N-[4-(3,4-dimethylphenyl)-2-(pivaloyloxymethyl)butyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2003.12.005

Reference yield:

: 503597-07-7
2-(3,4-dimethylphenethyl)-1,3-propanediol

: 503597-14-6
N-[4-(3,4-dimethylphenyl)-2-(pivaloyloxymethyl)butyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

2: 82 percent / PPh₃; diethyl azodicarboxylate; diphenylphosphoryl azide / tetrahydrofuran / 18 h / 20 °C

3: H₂ / Lindler's catalyst / ethanol / 2 h

4: 85 percent / CH₂Cl₂ / 20 °C

With pyridine; diphenylphosphoranyl azide; hydrogen; triphenylphosphine; diethylazodicarboxylate; Lindlar's catalyst; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.bmc.2003.12.005

Reference yield:

: 503597-09-9
4-(3,4-dimethylphenyl)-2-(hydroxymethyl)butyl pivalate

: 503597-14-6
N-[4-(3,4-dimethylphenyl)-2-(pivaloyloxymethyl)butyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / PPh₃; diethyl azodicarboxylate; diphenylphosphoryl azide / tetrahydrofuran / 18 h / 20 °C

2: H₂ / Lindler's catalyst / ethanol / 2 h

3: 85 percent / CH₂Cl₂ / 20 °C

With diphenylphosphoranyl azide; hydrogen; triphenylphosphine; diethylazodicarboxylate; Lindlar's catalyst; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.bmc.2003.12.005