Propanoic acid, 2,2-dimethyl-, 3-(3,4-dimethylphenyl)-2-[[[[[3-methoxy-4-(methoxymethoxy)phenyl]meth yl]amino]thioxomethyl]amino]propyl ester

Base Information

Chemical Name:Propanoic acid, 2,2-dimethyl-, 3-(3,4-dimethylphenyl)-2-[[[[[3-methoxy-4-(methoxymethoxy)phenyl]meth yl]amino]thioxomethyl]amino]propyl ester
CAS No.:503597-32-8
Molecular Formula:C27H38N2O5S
Molecular Weight:502.675
Hs Code.:

Propanoic acid, 2,2-dimethyl-,
3-(3,4-dimethylphenyl)-2-[[[[[3-methoxy-4-(methoxymethoxy)phenyl]meth
yl]amino]thioxomethyl]amino]propyl ester

Synonyms:

Suppliers and Price of Propanoic acid, 2,2-dimethyl-, 3-(3,4-dimethylphenyl)-2-[[[[[3-methoxy-4-(methoxymethoxy)phenyl]meth yl]amino]thioxomethyl]amino]propyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanoic acid, 2,2-dimethyl-, 3-(3,4-dimethylphenyl)-2-[[[[[3-methoxy-4-(methoxymethoxy)phenyl]meth yl]amino]thioxomethyl]amino]propyl ester

Chemical Property:

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Technology Process of Propanoic acid, 2,2-dimethyl-, 3-(3,4-dimethylphenyl)-2-[[[[[3-methoxy-4-(methoxymethoxy)phenyl]meth yl]amino]thioxomethyl]amino]propyl ester

There total 7 articles about Propanoic acid, 2,2-dimethyl-, 3-(3,4-dimethylphenyl)-2-[[[[[3-methoxy-4-(methoxymethoxy)phenyl]meth yl]amino]thioxomethyl]amino]propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2,2-dimethyl-propionic acid 2-amino-3-(3,4-dimethyl-phenyl)-propyl ester; compound with trifluoro-acetic acid

: 289903-62-4
4-[(methoxylmethyl)oxy]-3-methoxybenzyl isothiocyanate

: 503597-32-8
N-[3-(3,4-dimethylphenyl)-1-pivaloyloxy-2-propyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2003.12.005

Reference yield:

: 401573-46-4
ethyl 2-amino-3-(3,4-dimethylphenyl)propanoate

: 503597-32-8
N-[3-(3,4-dimethylphenyl)-1-pivaloyloxy-2-propyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / tetrahydrofuran / 16 h

2: 85 percent / LiAlH₄ / diethyl ether / 1 h / 20 °C

3: 99 percent / Et₃N; dimethylaminopyridine / CH₂Cl₂ / 1 h / 20 °C

4: CH₂Cl₂ / 3 h / 20 °C

5: 97 percent / Et₃N / CH₂Cl₂ / 20 °C

With dmap; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.bmc.2003.12.005

Reference yield:

: 401573-50-0
tert-butyl N-[2-(3,4-dimethylphenyl)-1-(hydroxymethyl)ethyl]carbamate

: 503597-32-8
N-[3-(3,4-dimethylphenyl)-1-pivaloyloxy-2-propyl]-N'-[3-methoxy-4-(methoxymethoxy)benzyl]thiourea

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Et₃N; dimethylaminopyridine / CH₂Cl₂ / 1 h / 20 °C

2: CH₂Cl₂ / 3 h / 20 °C

3: 97 percent / Et₃N / CH₂Cl₂ / 20 °C

With dmap; triethylamine; In dichloromethane;
DOI:10.1016/j.bmc.2003.12.005