[2,3,4,5-tetraacetyloxy-6-methylsulfanyl-6-(6-sulfanylidene-3H-purin-9-yl)hexyl] acetate

Base Information

Chemical Name:[2,3,4,5-tetraacetyloxy-6-methylsulfanyl-6-(6-sulfanylidene-3H-purin-9-yl)hexyl] acetate
CAS No.:74247-53-3
Molecular Formula:C₂₂H₂₈N₄O₁₀S₂
Molecular Weight:572.617
Hs Code.:
DSSTox Substance ID:DTXSID70408630
NSC Number:331773

Synonyms:NSC331773;74247-53-3;DTXSID70408630;NSC-331773

Suppliers and Price of [2,3,4,5-tetraacetyloxy-6-methylsulfanyl-6-(6-sulfanylidene-3H-purin-9-yl)hexyl] acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of [2,3,4,5-tetraacetyloxy-6-methylsulfanyl-6-(6-sulfanylidene-3H-purin-9-yl)hexyl] acetate

Chemical Property:

Vapor Pressure:3.91E-18mmHg at 25°C
Boiling Point:676°Cat760mmHg
Flash Point:362.7°C
Density:1.46g/cm³
XLogP3:0.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:13
Rotatable Bond Count:17
Exact Mass:572.12468545
Heavy Atom Count:38
Complexity:964

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OCC(C(C(C(C(N1C=NC2=C1NC=NC2=S)SC)OC(=O)C)OC(=O)C)OC(=O)C)OC(=O)C

Technology Process of [2,3,4,5-tetraacetyloxy-6-methylsulfanyl-6-(6-sulfanylidene-3H-purin-9-yl)hexyl] acetate

There total 1 articles about [2,3,4,5-tetraacetyloxy-6-methylsulfanyl-6-(6-sulfanylidene-3H-purin-9-yl)hexyl] acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 74247-51-1
2,3,4,5,6-penta-O-acetyl-1-(6-chloropurin-9-yl)-1-S-methyl-1-thio-D-glycero-D-ido-hexitol

: 17356-08-0
thiourea

: 74247-53-3
2,3,4,5,6-penta-O-acetyl-1-(1,6-dihydro-6-thioxopurin-9-yl)-1-S-methyl-1-thio-D-glycero-D-ido-hexitol

Guidance literature:: In ethanol; for 3h; Heating;
DOI:10.1016/S0008-6215(00)84863-6

Reference yield: 65.0%

: 74247-53-3
2,3,4,5,6-penta-O-acetyl-1-(1,6-dihydro-6-thioxopurin-9-yl)-1-S-methyl-1-thio-D-glycero-D-ido-hexitol

: 74247-54-4
1-(1,6-dihydro-6-thioxopurin-9-yl)-1-S-methyl-1-thio-D-glycero-D-ido-hexitol

Guidance literature:: With ammonia; In methanol; at 0 - 5 ℃; for 0.5h;
DOI:10.1016/S0008-6215(00)84863-6

Reference yield:

: 74247-53-3
2,3,4,5,6-penta-O-acetyl-1-(1,6-dihydro-6-thioxopurin-9-yl)-1-S-methyl-1-thio-D-glycero-D-ido-hexitol

: 74247-55-5
1-S-methyl-1-(6-methylthiopurin-9-yl)-1-thio-D-glycero-D-ido-hexitol

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / ammonia / methanol / 0.5 h / 0 - 5 °C

2: 67 percent / cc. ammonium hydroxide / H₂O / 1.5 h / Ambient temperature

With ammonium hydroxide; ammonia; In methanol; water;
DOI:10.1016/S0008-6215(00)84863-6