Benzenepentanethioic acid, b-hydroxy-, S-(phenylmethyl) ester

Base Information

Chemical Name:Benzenepentanethioic acid, b-hydroxy-, S-(phenylmethyl) ester
CAS No.:504414-61-3
Molecular Formula:C18H20O2S
Molecular Weight:300.422
Hs Code.:

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Chemical Property of Benzenepentanethioic acid, b-hydroxy-, S-(phenylmethyl) ester

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Technology Process of Benzenepentanethioic acid, b-hydroxy-, S-(phenylmethyl) ester

There total 2 articles about Benzenepentanethioic acid, b-hydroxy-, S-(phenylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 104-53-0
3-phenyl-propionaldehyde

: 61668-14-2
S-benzyl malonic acid half thioester

: 504414-61-3
3-hydroxy-5-phenylpentanethioic acid S-benzyl ester

Guidance literature:: With copper(II) 2-ethylhexanoate; 5-methoxy-1H-benzimidazole; In tetrahydrofuran; water; at 23 ℃; for 3.5h;
DOI:10.1021/ja029452x

Reference yield:

: 100-53-8
phenylmethanethiol

: 504414-61-3
3-hydroxy-5-phenylpentanethioic acid S-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl polyphosphate / CHCl₃; tetrahydrofuran / 40 h / 25 °C

2: 82 percent / Cu(2-ethylhexanoate)2; 5-methoxybenzimidazole / tetrahydrofuran; H₂O / 3.5 h / 23 °C

With copper(II) 2-ethylhexanoate; ethyl phosphate; 5-methoxy-1H-benzimidazole; In tetrahydrofuran; chloroform; water;
DOI:10.1021/ja029452x