1-(3-Bromopropyl)-3,6-dimethylpyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:1-(3-Bromopropyl)-3,6-dimethylpyrimidine-2,4(1H,3H)-dione
CAS No.:63550-50-5
Molecular Formula:C₉H₁₃BrN₂O₂
Molecular Weight:261.118
Hs Code.:
DSSTox Substance ID:DTXSID90382685
Nikkaji Number:J458.072I
Wikidata:Q82174054

Synonyms:BAS 01054099;DTXSID90382685;AKOS000565519;63550-50-5;SR-01000314875;SR-01000314875-1;1-(3-Bromopropyl)-3,6-dimethylpyrimidine-2,4(1H,3H)-dione

Suppliers and Price of 1-(3-Bromopropyl)-3,6-dimethylpyrimidine-2,4(1H,3H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1-(3-Bromopropyl)-3,6-dimethylpyrimidine-2,4(1H,3H)-dione

Chemical Property:

Vapor Pressure:0.000245mmHg at 25°C
Boiling Point:324.5°Cat760mmHg
Flash Point:150°C
Density:1.449g/cm³
XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:260.01604
Heavy Atom Count:14
Complexity:289

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=O)N(C(=O)N1CCCBr)C

Technology Process of 1-(3-Bromopropyl)-3,6-dimethylpyrimidine-2,4(1H,3H)-dione

There total 3 articles about 1-(3-Bromopropyl)-3,6-dimethylpyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 76889-80-0
3,6-dimethyl-1-(γ-hydroxypropyl)uracil

: 63550-50-5
1-(3-bromoprop-1-y)-3,6-dimethyluracil

Guidance literature:: With hydrogen bromide; at 130 - 140 ℃; for 3h;
DOI:10.1002/jhet.5570280817

Reference yield:

: 10128-60-6
3,6-dimethyl-2H-1,3-oxazine-2,4(3H)-dione

: 63550-50-5
1-(3-bromoprop-1-y)-3,6-dimethyluracil

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / CH₂Cl₂ / 1 h / Ambient temperature

2: 91 percent / aq. HBr / 3 h / 130 - 140 °C

With hydrogen bromide; In dichloromethane;
DOI:10.1002/jhet.5570280817