Ici 180080

Base Information

• Chemical Name: Ici 180080
• CAS No.: 89425-94-5
• Molecular Formula: C₁₉H₂₆O₅
• Molecular Weight: 334.412

Synonyms:

Chemical Property of Ici 180080

Chemical Property:

• PSA: 75.99000
• LogP: 4.03360

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ici 180080

There total 2 articles about Ici 180080 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

5(Z)-7-<2,2-dimethyl-4-(2-methoxyphenyl)-1,3-dioxan-cis-5-yl>heptenoic acid → (5Z)-7-<2,2-dimethyl-4-(2-hydroxyphenyl)-1,3-dioxan-cis-5-yl>heptenoic acid (89425-94-5,105846-98-8)

Guidance literature:

With sodium thioethoxide; In N,N-dimethyl-formamide; for 1.16667h; Heating;

DOI:10.1111/j.2042-7158.1986.tb03117.x

Reference yield:

(4,5-cis)5-allyl-2,2-dimethyl-4-(2-methoxyphenyl)-1,3-dioxane → (5Z)-7-<2,2-dimethyl-4-(2-hydroxyphenyl)-1,3-dioxan-cis-5-yl>heptenoic acid (89425-94-5,105846-98-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 57 percent / potassium t-butoxide / tetrahydrofuran / 1.5 h / 0 - 5 °C

2: 74 percent / 0.5 M sodium thioethoxide / dimethylformamide / 1.17 h / Heating

With sodium thioethoxide; potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1111/j.2042-7158.1986.tb03117.x

Reference yield: 78.0%

(5Z)-7-<2,2-dimethyl-4-(2-hydroxyphenyl)-1,3-dioxan-cis-5-yl>heptenoic acid (89425-94-5,105846-98-8) + methyl iodide (74-88-4) → methyl-5(Z)-7-<2,2-dimethyl-4-(2-hydroxyphenyl)-1,3-dioxan-cis-5-yl>heptenoate

Guidance literature:

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; potassium carbonate; for 2h; Ambient temperature;

DOI:10.1111/j.2042-7158.1986.tb03117.x

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