Benzene, 1-(2-propenyl)-2-(2-propynyloxy)-

Base Information

Chemical Name:Benzene, 1-(2-propenyl)-2-(2-propynyloxy)-
CAS No.:51230-30-9
Molecular Formula:C12H12O
Molecular Weight:172.227
Hs Code.:
DSSTox Substance ID:DTXSID10458937
Nikkaji Number:J1.075.583B
Wikidata:Q82282511

Synonyms:51230-30-9;Benzene, 1-(2-propenyl)-2-(2-propynyloxy)-;Propargyl(2-allylphenyl) ether;DTXSID10458937

Suppliers and Price of Benzene, 1-(2-propenyl)-2-(2-propynyloxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-(2-propenyl)-2-(2-propynyloxy)-

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:172.088815002
Heavy Atom Count:13
Complexity:198

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCC1=CC=CC=C1OCC#C

Technology Process of Benzene, 1-(2-propenyl)-2-(2-propynyloxy)-

There total 2 articles about Benzene, 1-(2-propenyl)-2-(2-propynyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 106-96-7
propargyl bromide

: 1745-81-9
o-Allylphenol

: 51230-30-9
1-allyl-2-prop-2-ynyloxy-benzene

Guidance literature:: With potassium carbonate; In acetone; for 4h; Heating;
DOI:10.1016/j.tetlet.2005.12.131 DOI:10.1016/j.tet.2007.08.072

Reference yield:

: 1746-13-0
allyl phenyl ether

: 51230-30-9
1-allyl-2-prop-2-ynyloxy-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / K₂CO₃ / acetone / 4 h / Heating

With potassium carbonate; In acetone; 1: Claisen rearrangement;
DOI:10.1016/j.tetlet.2005.12.131

Reference yield: 94.0%

: 541-41-3
chloroformic acid ethyl ester

: 51230-30-9
1-allyl-2-prop-2-ynyloxy-benzene

: 4-(2-allyl-phenoxy)-but-2-ynoic acid ethyl ester

Guidance literature:: 1-allyl-2-prop-2-ynyloxy-benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -40 ℃; for 1h;

chloroformic acid ethyl ester; In tetrahydrofuran; hexane; at -40 ℃; for 1h; Further stages.;
DOI:10.1016/j.tet.2007.08.072