2-Benzyl-3-methylcyclohex-2-en-1-one

Base Information

Chemical Name:2-Benzyl-3-methylcyclohex-2-en-1-one
CAS No.:5134-46-3
Molecular Formula:C14H16O
Molecular Weight:200.28
Hs Code.:
DSSTox Substance ID:DTXSID90569176
Wikidata:Q82456271

Synonyms:2-Benzyl-3-methylcyclohex-2-en-1-one;5134-46-3;DTXSID90569176

Suppliers and Price of 2-Benzyl-3-methylcyclohex-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-Benzyl-3-methylcyclohex-2-en-1-one

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:200.120115130
Heavy Atom Count:15
Complexity:269

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=O)CCC1)CC2=CC=CC=C2

Technology Process of 2-Benzyl-3-methylcyclohex-2-en-1-one

There total 10 articles about 2-Benzyl-3-methylcyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1-benzyl-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one

: 5134-46-3
2-benzyl-3-methylcyclohex-2-en-1-one

Guidance literature:: With bis(cyclopentadienyl)titanium (III) chloride; In tetrahydrofuran; at 20 ℃; for 0.75h; Further Variations:; Reaction partners; Product distribution;

Reference yield:

: 17939-02-5
rac.-2-Benzyl-3-methyl-4-carbethoxy-Δ²-cyclohexenon-(1)

: 5134-46-3
2-benzyl-3-methylcyclohex-2-en-1-one

Guidance literature:: With potassium hydroxide; In ethanol;
DOI:10.1016/S0040-4020(01)82464-9

Reference yield:

: 100-39-0
benzyl bromide

: 140710-03-8
2-Iodo-3-methyl-2-cyclohexen-1-one

: 5134-46-3
2-benzyl-3-methylcyclohex-2-en-1-one

Guidance literature:: benzyl bromide; With ethylene dibromide; zinc; In tetrahydrofuran; at 0 ℃; for 3h;

2-Iodo-3-methyl-2-cyclohexen-1-one; With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; N,N-dimethyl-formamide; at 23 ℃; for 2h;
DOI:10.1016/S0040-4020(00)00864-4