5-Pyrimidinecarboxylic acid, 1,2,3,6-tetrahydro-4-methyl-2-oxo-6-thioxo-

Base Information

• Chemical Name: 5-Pyrimidinecarboxylic acid, 1,2,3,6-tetrahydro-4-methyl-2-oxo-6-thioxo-
• CAS No.: 51622-66-3
• Molecular Formula: C6H6N2O3S
• Molecular Weight: 186.18800
• Mol file: 51622-66-3.mol

Synonyms:6-Methyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid;1,2,3,4-Tetrahydro-6-methyl-2-oxo-4-thioxo-5-pyrimidinecarboxylic acid;

Chemical Property of 5-Pyrimidinecarboxylic acid, 1,2,3,6-tetrahydro-4-methyl-2-oxo-6-thioxo-

Chemical Property:

• PSA: 122.11000
• LogP: 0.47750

Purity/Quality:

99% ^*data from raw suppliers

6-Methyl-2-oxo-4-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylic acid 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Pyrimidinecarboxylic acid, 1,2,3,6-tetrahydro-4-methyl-2-oxo-6-thioxo-

There total 1 articles about 5-Pyrimidinecarboxylic acid, 1,2,3,6-tetrahydro-4-methyl-2-oxo-6-thioxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-Hydroxy-4-mercapto-6-methylpyrimidine-5-carboxylic acid (51622-66-3)

Guidance literature:

Ester III, NaOH;

Reference yield: 85.0%

6-methyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid (51622-66-3) + 3,5-Dichloroaniline (626-43-7) → 5-3',5'-Dichlorophenylcarbamoyl-1,2,3,4-tetrahydro-6-methyl-2-oxo-4-thiopyrimidine (124881-47-6)

Guidance literature:

With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 60 ℃;

DOI:10.1002/ardp.19893221006

Reference yield: 75.0%

6-methyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid (51622-66-3) + m,p-dichloroaniline (95-76-1) → 6-Methyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid (3,4-dichloro-phenyl)-amide (170963-76-5)

Guidance literature:

With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; Ambient temperature;

Downstream raw materials:

5-Cyclohexylcarbamoyl-2-hydroxy-4-mercapto-6-methylpyrimidine

2-Hydroxy-4-(2-hydroxy-ethylamino)-6-methyl-pyrimidine-5-carboxylic acid cyclohexylamide

8-Cyclohexylcarbamoyl-1H-7-methyl-5-oxo-2,3-dihydroimidazo<1,2-c>pyrimidine hydrochloride

1,2,3,4-Tetrahydro-6-methyl-2-oxo-4-thio-5-p-tolylcarbamoylpyrimidine

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