4-Nitrostyrylsulfonamide

Base Information

Chemical Name:4-Nitrostyrylsulfonamide
CAS No.:52147-91-8
Molecular Formula:C8H8N2O4S
Molecular Weight:228.229
Hs Code.:
DSSTox Substance ID:DTXSID40705542
Mol file:52147-91-8.mol

Synonyms:2-(4-Nitrophenyl)ethene-1-sulfonamide;52147-91-8;4-nitrostyrylsulfonamide;DTXSID40705542;AAWSZAQEVCTOLT-UHFFFAOYSA-N

Suppliers and Price of 4-Nitrostyrylsulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of 4-Nitrostyrylsulfonamide

Chemical Property:

XLogP3:0.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:228.02047791
Heavy Atom Count:15
Complexity:344

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C=CS(=O)(=O)N)[N+](=O)[O-]

Technology Process of 4-Nitrostyrylsulfonamide

There total 5 articles about 4-Nitrostyrylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: C₁₃H₁₆N₂O₆S

: 52147-91-8
(E)-4-nitrophenylethenesulfonamide

Guidance literature:: In dimethyl sulfoxide; at 80 ℃; for 8h;
DOI:10.1039/d0cc00220h

Reference yield:

: 52148-00-2
trans-2-(p-nitrophenyl)ethenesulfonyl chloride

: 52147-91-8
(E)-4-nitrophenylethenesulfonamide

Guidance literature:: With ammonia;
DOI:10.1021/ja01213a030

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 52147-91-8
(E)-4-nitrophenylethenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

1.2: 0 - 20 °C / Inert atmosphere; Schlenk technique

2.1: dimethyl sulfoxide / 8 h / 80 °C

With sodium hydride; In dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/d0cc00220h