1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE

Base Information

Chemical Name:1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE
CAS No.:52178-73-1
Molecular Formula:C11H12Br2O
Molecular Weight:320.024
Hs Code.:
Mol file:52178-73-1.mol

Synonyms:p-(2,2-dibromo-1-methylcyclopropyl)anisole;1,1-dibromo-2-methyl-2-p-methoxyphenylcyclopropane;

Suppliers and Price of 1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE 95.00%
10G
$ 2483.25

American Custom Chemicals Corporation
1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE 95.00%
5G
$ 1697.85

American Custom Chemicals Corporation
1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE 95.00%
1G
$ 1062.60

Total 3 raw suppliers

Chemical Property of 1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE

Chemical Property:

PSA：9.23000
LogP:3.84270

Purity/Quality:

99% ^*data from raw suppliers

1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE

There total 2 articles about 1-(2,2-DIBROMO-1-METHYL-CYCLOPROPYL)-4-METHOXY-BENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 75-25-2
Bromoform

: 1712-69-2
1-isopropenyl-4-methoxybenzene

: 52178-73-1
1-(2,2-dibromo-1-methylcyclopropyl)-4-methoxybenzene

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; water; at 30 - 35 ℃; for 48h;
DOI:10.1016/j.tet.2008.06.087

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 52178-73-1
1-(2,2-dibromo-1-methylcyclopropyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C

1.2: 16 h / 0 - 20 °C

2.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / dichloromethane; water / 30 - 35 °C

With potassium tert-butylate; N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/adsc.201600304

Reference yield: 75.0%

: 52178-73-1
1-(2,2-dibromo-1-methylcyclopropyl)-4-methoxybenzene

: 87959-49-7
1-(buta-2,3-dien-2-yl)-4-methoxybenzene

Guidance literature:: With ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201706798