3,3-Dimethyl-11-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Base Information

Chemical Name:3,3-Dimethyl-11-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one
CAS No.:37587-36-3
Molecular Formula:C21H22N2O
Molecular Weight:318.418
Hs Code.:
NSC Number:186217
Nikkaji Number:J1.188.151C
ChEMBL ID:CHEMBL2180492
Mol file:37587-36-3.mol

Synonyms:37587-36-3;3,3-Dimethyl-11-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one;NSC186217;NSC 186217;CHEMBL2180492;9,9-dimethyl-6-phenyl-6,8,10,11-tetrahydro-5H-benzo[b][1,4]benzodiazepin-7-one;3,3-Dimethyl-11-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo(b,e)(1,4)diazepin-1-one;Enamine_003299;Cambridge id 5325930;Oprea1_003182;Oprea1_409964;Oprea1_527083;CBDivE_016161;SCHEMBL13704121;HMS1403F21;HMS1584F12;BDBM50485889;STK741937;STK868323;AKOS000558745;AKOS005524429;AKOS022088566;NSC-186217;AJ-077/33270030;Z56849241;3,3-dimethyl-11-phenyl-2,3,4,5,10,11-hexahydrodibenzo[b,e]-1,4-diazepin-1-one;3,3-dimethyl-11-phenyl-3,4,10,11-tetrahydro-2H-dibenzo[b,e][1,4]diazepin-1-ol

Suppliers and Price of 3,3-Dimethyl-11-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 3,3-Dimethyl-11-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Chemical Property:

Vapor Pressure:4.14E-10mmHg at 25°C
Boiling Point:499.5°Cat760mmHg
Flash Point:170.8°C
PSA：41.13000
Density:1.19g/cm³
LogP:5.18450
XLogP3:4.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:318.173213330
Heavy Atom Count:24
Complexity:530

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CC2=C(C(NC3=CC=CC=C3N2)C4=CC=CC=C4)C(=O)C1)C

Technology Process of 3,3-Dimethyl-11-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

There total 14 articles about 3,3-Dimethyl-11-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 100-52-7
benzaldehyde

: 126-81-8
dimedone

: 95-54-5
1,2-diamino-benzene

: 37587-36-3
3,3-dimethyl-11-phenyl-2,3,4,5,10,11-hexahydro-1H-dibenzo<1,4>diazepin-1-one

Guidance literature:: With H₅PW₁₁CuO₃₉ polyoxometalate immobilized on diamine-functionalized silica-coated CoFe₂O₄ magnetite nanoparticles; In neat (no solvent); at 80 ℃; for 0.166667h; Green chemistry;
DOI:10.1016/j.poly.2019.03.046