Dimethyl 3,4-diaminophthalate

Base Information

Chemical Name:Dimethyl 3,4-diaminophthalate
CAS No.:52412-60-9
Molecular Formula:C10H12N2O4
Molecular Weight:224.216
Hs Code.:
DSSTox Substance ID:DTXSID301179611
Mol file:52412-60-9.mol

Synonyms:dimethyl 3,4-diaminophthalate;SCHEMBL8953053;ROPYKWJBZRXADC-UHFFFAOYSA-N;DTXSID301179611;52412-60-9;1,2-Benzenedicarboxylic acid, 3,4-diamino-, 1,2-dimethyl ester

Suppliers and Price of Dimethyl 3,4-diaminophthalate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl 3,4-diaminophthalate

Chemical Property:

XLogP3:0.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:224.07970687
Heavy Atom Count:16
Complexity:282

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC(=O)C1=C(C(=C(C=C1)N)N)C(=O)OC

Technology Process of Dimethyl 3,4-diaminophthalate

There total 6 articles about Dimethyl 3,4-diaminophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 610-27-5
4-nitrophthalic acid

: 52412-60-9
dimethyl 3,4-diaminophthalate

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid / 10 h / Reflux

2: hydrogen; palladium on activated charcoal / methanol / 20 °C

3: toluene / 4 h / 80 °C

4: nitric acid / 0 - 5 °C

5: sulfuric acid / 0.5 h / 20 °C

6: hydrogen; palladium on activated charcoal / methanol / 20 °C

With sulfuric acid; palladium on activated charcoal; hydrogen; nitric acid; In methanol; toluene;
DOI:10.1016/j.dyepig.2014.08.009

Reference yield:

: 51832-56-5
3,4-dimethoxycarbonylacetanilide

: 52412-60-9
dimethyl 3,4-diaminophthalate

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid / 0 - 5 °C

2: sulfuric acid / 0.5 h / 20 °C

3: hydrogen; palladium on activated charcoal / methanol / 20 °C

With sulfuric acid; palladium on activated charcoal; hydrogen; nitric acid; In methanol;
DOI:10.1016/j.dyepig.2014.08.009

Reference yield:

: 52412-56-3
dimethyl 4-acetamido-3-nitrophthalate

: 52412-60-9
dimethyl 3,4-diaminophthalate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 0.5 h / 20 °C

2: hydrogen; palladium on activated charcoal / methanol / 20 °C

With sulfuric acid; palladium on activated charcoal; hydrogen; In methanol;
DOI:10.1016/j.dyepig.2014.08.009