Dimethyl 4-acetamido-5-nitrophthalate

Base Information

Chemical Name:Dimethyl 4-acetamido-5-nitrophthalate
CAS No.:52412-56-3
Molecular Formula:C12H12N2O7
Molecular Weight:296.236
Hs Code.:
DSSTox Substance ID:DTXSID301334265
Nikkaji Number:J1.453.312E

Synonyms:dimethyl 4-acetamido-5-nitrophthalate;52412-56-3;SCHEMBL8954112;ZKSCTCPUUGZZAG-UHFFFAOYSA-N;DTXSID301334265

Suppliers and Price of Dimethyl 4-acetamido-5-nitrophthalate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl 4-acetamido-5-nitrophthalate

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:5
Exact Mass:296.06445073
Heavy Atom Count:21
Complexity:445

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)NC1=C(C=C(C(=C1)C(=O)OC)C(=O)OC)[N+](=O)[O-]

Technology Process of Dimethyl 4-acetamido-5-nitrophthalate

There total 5 articles about Dimethyl 4-acetamido-5-nitrophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51832-56-5
3,4-dimethoxycarbonylacetanilide

: 52412-55-2
dimethyl 4-acetamido-5-nitrophthalate

: 52412-56-3
dimethyl 4-acetamido-3-nitrophthalate

Guidance literature:: With nitric acid; In dichloromethane;

Reference yield:

: 610-22-0
dimethyl 4-nitrophthalate

: 52412-56-3
dimethyl 4-acetamido-3-nitrophthalate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium on activated charcoal / methanol / 20 °C

2: toluene / 4 h / 80 °C

3: nitric acid / 0 - 5 °C

With palladium on activated charcoal; hydrogen; nitric acid; In methanol; toluene;
DOI:10.1016/j.dyepig.2014.08.009

Reference yield:

: 610-27-5
4-nitrophthalic acid

: 52412-56-3
dimethyl 4-acetamido-3-nitrophthalate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 10 h / Reflux

2: hydrogen; palladium on activated charcoal / methanol / 20 °C

3: toluene / 4 h / 80 °C

4: nitric acid / 0 - 5 °C

With sulfuric acid; palladium on activated charcoal; hydrogen; nitric acid; In methanol; toluene;
DOI:10.1016/j.dyepig.2014.08.009