(E)-(4-Methoxyphenyl)diazene-1-carbonitrile

Base Information

Chemical Name:(E)-(4-Methoxyphenyl)diazene-1-carbonitrile
CAS No.:52512-40-0
Molecular Formula:C8H7N3O
Molecular Weight:161.16100
Hs Code.:
DSSTox Substance ID:DTXSID70502884
Mol file:52512-40-0.mol

Synonyms:52512-40-0;(E)-(4-Methoxyphenyl)diazene-1-carbonitrile;SCHEMBL14831276;DTXSID70502884

Suppliers and Price of (E)-(4-Methoxyphenyl)diazene-1-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-(4-Methoxyphenyl)diazene-1-carbonitrile

Chemical Property:

PSA：57.74000
LogP:2.25998
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:161.058911855
Heavy Atom Count:12
Complexity:198

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N=NC#N

Technology Process of (E)-(4-Methoxyphenyl)diazene-1-carbonitrile

There total 8 articles about (E)-(4-Methoxyphenyl)diazene-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 459-64-3
4-methoxybenzenediazonium tetrafluoroborate

: 151-50-8
potassium cyanide

: 52512-40-0
(E)-4-methoxybenzenediazocyanide

Guidance literature:: With 18-crown-6 ether; In dichloromethane; for 5h; Ambient temperature;
DOI:10.1021/ja00366a030

Reference yield:

: 52512-40-0
(E)-4-methoxybenzenediazocyanide

: 828-16-0,52512-40-0,58468-78-3
C₈H₇N₃O^(1-)

Guidance literature:: With potassium; In tetrahydrofuran; Title compound not separated from byproducts;

Reference yield:

: 104-94-9
4-methoxy-aniline

: 52512-40-0
(E)-4-methoxybenzenediazocyanide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / fluoroboric acid; sodium nitrite / H₂O / 0.25 h / 0 - 5 °C

2.1: H₂O / 0 °C

2.2: H₂O / Heating

With tetrafluoroboric acid; sodium nitrite; In water;
DOI:10.1039/b200747a