Thiazole, 4,5-dihydro-2-[[1-(phenylmethyl)-2-propenyl]thio]-

Base Information

Chemical Name:Thiazole, 4,5-dihydro-2-[[1-(phenylmethyl)-2-propenyl]thio]-
CAS No.:52534-82-4
Molecular Formula:C₁₃H₁₅NS₂
Molecular Weight:249.401
Hs Code.:
Mol file:52534-82-4.mol

Synonyms:

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Chemical Property of Thiazole, 4,5-dihydro-2-[[1-(phenylmethyl)-2-propenyl]thio]-

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Technology Process of Thiazole, 4,5-dihydro-2-[[1-(phenylmethyl)-2-propenyl]thio]-

There total 1 articles about Thiazole, 4,5-dihydro-2-[[1-(phenylmethyl)-2-propenyl]thio]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52534-82-4
2-(1-benzyl-allylsulfanyl)-4,5-dihydro-thiazole

Guidance literature:: 2-Allythio-2-thiazolin, 1.) Li-butyl,2.) Benzylbromid;

Reference yield: 73.0%

: 52534-82-4
2-(1-benzyl-allylsulfanyl)-4,5-dihydro-thiazole

: 4226-01-1
tri-n-butyltin lithium

: 75950-62-8
PhCH₂CHCHCH₂(tributylstannyl)

Guidance literature:: With copper(I) bromide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; addn. of a soln. of tributylstannyllithium in THF to a mixt. of the thiobutene and CuBr in THF/HMPT at 0°C under Ar with stirring for 1 h; quenching with phosphate buffer soln. (pH 7), extn. with CH2Cl2, drying over Na2SO4, concg. under reduced pressure, chromy. on silica gel (hexane), IR, NMR;
DOI:10.1246/cl.1987.1967