Silane, [5-(2-propenyl)-1,3-phenylene]bis[trimethyl-

Base Information

Chemical Name:Silane, [5-(2-propenyl)-1,3-phenylene]bis[trimethyl-
CAS No.:528577-22-2
Molecular Formula:C15H26Si2
Molecular Weight:262.542
Hs Code.:
DSSTox Substance ID:DTXSID10476833
Mol file:528577-22-2.mol

Synonyms:528577-22-2;Silane, [5-(2-propenyl)-1,3-phenylene]bis[trimethyl-;DTXSID10476833

Suppliers and Price of Silane, [5-(2-propenyl)-1,3-phenylene]bis[trimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, [5-(2-propenyl)-1,3-phenylene]bis[trimethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:262.15730390
Heavy Atom Count:17
Complexity:235

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C[Si](C)(C)C1=CC(=CC(=C1)CC=C)[Si](C)(C)C

Technology Process of Silane, [5-(2-propenyl)-1,3-phenylene]bis[trimethyl-

There total 2 articles about Silane, [5-(2-propenyl)-1,3-phenylene]bis[trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 106-95-6
allyl bromide

: 81500-92-7
3,5-Bis-trimethylsilyl-bromobenzene

: 528577-22-2
1-allyl-3,5-bis(trimethylsilyl)benzene

Guidance literature:: 3,5-Bis-trimethylsilyl-bromobenzene; With iodine; magnesium; In tetrahydrofuran; for 6h; Heating;

allyl bromide; palladium dichloride; In tetrahydrofuran; at 0 - 20 ℃; Further stages.;
DOI:10.1039/b306601k

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 528577-22-2
1-allyl-3,5-bis(trimethylsilyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / diethyl ether / 1 h / -78 °C

1.2: 99 percent / diethyl ether / -78 - 20 °C

2.1: Mg; I₂ / tetrahydrofuran / 6 h / Heating

2.2: 92 percent / PdCl₂ / tetrahydrofuran / 0 - 20 °C

With n-butyllithium; iodine; magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1039/b306601k

Reference yield:

: 528577-22-2
1-allyl-3,5-bis(trimethylsilyl)benzene

: 634598-09-7
1-[3-(4-bromophenyl)propyl]-3,5-bis(trimethylsilyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 48 h / 20 °C

2: 86 percent / aq. NaOH / Pd(PPh₃)4 / tetrahydrofuran / 3 h / 20 °C

With sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran;
DOI:10.1039/b306601k