Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(2-phenyl-1-propenylidene)-

Base Information

Chemical Name:Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(2-phenyl-1-propenylidene)-
CAS No.:53097-53-3
Molecular Formula:C15H23NSi
Molecular Weight:245.44
Hs Code.:
Mol file:53097-53-3.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(2-phenyl-1-propenylidene)-

Chemical Property:

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Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(2-phenyl-1-propenylidene)-

There total 2 articles about Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(2-phenyl-1-propenylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1823-91-2
1-phenylethyl cyanide

: 53097-53-3
1-(2,3-dimethylbutan-2-yl)-1,1-dimethyl-N-(2-phenylprop-1-en-1-ylidene)silanamine

Guidance literature:: 1-phenylethyl cyanide; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h;

tert-butyldimethylsilyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1002/anie.200461886

Reference yield:

: 53097-53-3
1-(2,3-dimethylbutan-2-yl)-1,1-dimethyl-N-(2-phenylprop-1-en-1-ylidene)silanamine

Guidance literature:: 2-Phenylpropionitril: 1) n-BuLi/i-Pr2NH 2) t-Butyldimethylchlorsilan (Tab.I);
DOI:10.1021/jo00932a028

Reference yield: 98.0%

: 53097-53-3
1-(2,3-dimethylbutan-2-yl)-1,1-dimethyl-N-(2-phenylprop-1-en-1-ylidene)silanamine

: 1426931-85-2
tert-butyl (1-benzyl-7-fluoro-2-oxoindolin-3-ylidene)carbamate

: tert-butyl (1-benzyl-3-(1-cyano-1-phenylethyl)-7-fluoro-2-oxoindolin-3-yl)carbamate

Guidance literature:: With C₃₁H₄₀N₄O₄; zinc trifluoromethanesulfonate; In tetrahydrofuran; at -45 ℃; for 12h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201408730