DANSYLAMIDOETHYL MERCAPTAN

Base Information

Chemical Name:DANSYLAMIDOETHYL MERCAPTAN
CAS No.:5354-61-0
Molecular Formula:C14H18N2O2S2
Molecular Weight:310.441
Hs Code.:2935009090
DSSTox Substance ID:DTXSID20409591
Nikkaji Number:J2.320.415K
Wikidata:Q82215466
Mol file:5354-61-0.mol

Synonyms:2-(5-Dimethylaminonaphth-1-ylsulfonamido)ethyl Mercaptan;Dansylamidoethyl Mercaptan;N-(2-mercaptoethyl)-dansylamide;

Suppliers and Price of DANSYLAMIDOETHYL MERCAPTAN

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Dansylamidoethyl Mercaptan
10mg
$ 403.00

TRC
DansylamidoethylMercaptan
25mg
$ 250.00

Medical Isotopes, Inc.
DansylamidoethylMercaptan
50 mg
$ 1880.00

Biosynth Carbosynth
Dansylamidoethyl mercaptan
50 mg
$ 660.50

Biosynth Carbosynth
Dansylamidoethyl mercaptan
25 mg
$ 363.50

Biosynth Carbosynth
Dansylamidoethyl mercaptan
10 mg
$ 199.90

Biosynth Carbosynth
Dansylamidoethyl mercaptan
5 mg
$ 109.90

Biosynth Carbosynth
Dansylamidoethyl mercaptan
100 mg
$ 1202.00

American Custom Chemicals Corporation
DANSYLAMIDOETHYL MERCAPTAN 95.00%
100MG
$ 1593.90

American Custom Chemicals Corporation
DANSYLAMIDOETHYL MERCAPTAN 95.00%
10MG
$ 704.55

Total 8 raw suppliers

Chemical Property of DANSYLAMIDOETHYL MERCAPTAN

Chemical Property:

Melting Point:106-108°C
PSA：96.59000
LogP:3.58560
Storage Temp.:Amber Vial, -20?C Freezer, Under Inert Atmosphere
Solubility.:Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly, Heated)
XLogP3:2.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:310.08097017
Heavy Atom Count:20
Complexity:406

Purity/Quality:

97% ^*data from raw suppliers

Dansylamidoethyl Mercaptan ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C)C1=CC=CC2=C1C=CC=C2S(=O)(=O)NCCS
Uses Fluorescence: max. Abs. 335nm; max. Em. 526nm; e x 10-3: 4.1

Technology Process of DANSYLAMIDOETHYL MERCAPTAN

There total 9 articles about DANSYLAMIDOETHYL MERCAPTAN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 881013-37-2
N,N’-(disulfanediylbis(ethane-2,1-diyl))bis(5-(dimethylamino)naphthalene-1-sulfonamide)

: 5354-61-0
5-(dimethylamino)-N-(2-sulfanylethyl)naphthalene-1-sulfonamide

Guidance literature:: With zinc; In ethanol; at 20 ℃; for 16h;
DOI:10.1002/anie.201603921

Reference yield:

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 5354-61-0
5-(dimethylamino)-N-(2-sulfanylethyl)naphthalene-1-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 20 °C

2: Et₃N / CH₂Cl₂ / -20 - 0 °C

3: acetone / 20 °C

4: DIBALH / CH₂Cl₂; hexane / -78 °C

With diisobutylaluminium hydride; triethylamine; In hexane; dichloromethane; acetone;
DOI:10.1021/jo015658p