(E)-Diazene-1,2-dicarbonitrile

Base Information

• Chemical Name: (E)-Diazene-1,2-dicarbonitrile
• CAS No.: 1557-57-9
• Molecular Formula: C₂N₄
• Molecular Weight: 80.0488
• DSSTox Substance ID: DTXSID40516034
• Nikkaji Number: J1.440.661A
• Mol file: 1557-57-9.mol

Synonyms:azocyanide;(E)-Diazene-1,2-dicarbonitrile;1557-57-9;DTXSID40516034

Chemical Property of (E)-Diazene-1,2-dicarbonitrile

Chemical Property:

• XLogP3: 0.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 80.012296017
• Heavy Atom Count: 6
• Complexity: 119

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Safety Statements: An explosive sensitive to shock or heating in a closed container. Upon decom"> − and NOx. See also CYANIDE." target="_blank">An explosive sensitive to shock or heating in a closed container. Upon decom

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(#N)N=NC#N

Technology Process of (E)-Diazene-1,2-dicarbonitrile

There total 6 articles about (E)-Diazene-1,2-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyanogen azide (764-05-6) → Dicyano-diazene (1557-57-9)

Guidance literature:

In gas; pyrolysis at 200°C; N3CN is hazardous to handle and may detonate vigorously on impact or warming, therefore only small amounts of NCNNCN can be prepared;

DOI:10.1021/ja01086a054

Reference yield:

cyanonitrene (1884-64-6,2669-76-3) → Dicyano-diazene (1557-57-9)

Guidance literature:

In methanol; at 0 - 10 ℃;

DOI:10.1021/jo00146a005

Reference yield:

CYANAMID (420-04-2) → Dicyano-diazene (1557-57-9)

Guidance literature:

With tert-butylhypochlorite; sodium; Multistep reaction; 1.) methanol, -50 deg C, 2.) room temperature;

DOI:10.1016/S0040-4039(01)82991-9

upstream raw materials:

CYANAMID

cyanonitrene

ethanedinitrile

oxygen