2,2-Dimethyl-5,6-dinitro-1,3-benzodioxole

Base Information

Chemical Name:2,2-Dimethyl-5,6-dinitro-1,3-benzodioxole
CAS No.:54186-71-9
Molecular Formula:C9H8N2O6
Molecular Weight:240.17000
Hs Code.:
DSSTox Substance ID:DTXSID00407777
Wikidata:Q82213116

Synonyms:2,2-dimethyl-5,6-dinitro-1,3-benzodioxole;54186-71-9;Oprea1_020571;SCHEMBL8313566;DTXSID00407777;PMYSRAAYCZPNHT-UHFFFAOYSA-N;AKOS005737774;AE-562/12222263

Suppliers and Price of 2,2-Dimethyl-5,6-dinitro-1,3-benzodioxole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,2-DIMETHYL-5,6-DINITRO-1,3-BENZODIOXOLE 95.00%
5MG
$ 503.34

Total 0 raw suppliers

Chemical Property of 2,2-Dimethyl-5,6-dinitro-1,3-benzodioxole

Chemical Property:

PSA：110.10000
LogP:3.05670
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:0
Exact Mass:240.03823598
Heavy Atom Count:17
Complexity:314

Purity/Quality:: 2,2-DIMETHYL-5,6-DINITRO-1,3-BENZODIOXOLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(OC2=C(O1)C=C(C(=C2)[N+](=O)[O-])[N+](=O)[O-])C

Technology Process of 2,2-Dimethyl-5,6-dinitro-1,3-benzodioxole

There total 5 articles about 2,2-Dimethyl-5,6-dinitro-1,3-benzodioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 54186-68-4
2,2-dimethyl-5-nitro-1,3-benzodioxole

: 54186-71-9
2,2-dimethyl-5,6-nitro[1,3]benzodioxole

Guidance literature:: With nitric acid; acetic acid; at 10 - 20 ℃; for 0.75h;

Reference yield: 85.0%

: 54186-71-9
2,2-dimethyl-5,6-nitro[1,3]benzodioxole

Guidance literature:: With nitric acid; acetic acid; at 0 - 20 ℃; for 0.5h;

With sulfuric acid; nitric acid; acetic acid; at 20 - 80 ℃; for 2.5h; Cooling with ice;

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 54186-71-9
2,2-dimethyl-5,6-nitro[1,3]benzodioxole

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / benzene / 48 h / Reflux; Molecular sieve

2: acetic acid; nitric acid / 0.75 h / 10 - 20 °C

3: acetic acid; nitric acid / 0.75 h / 10 - 20 °C

With nitric acid; toluene-4-sulfonic acid; acetic acid; In benzene;