5H,6H,7H-benzo[c]carbazole

Base Information

• Chemical Name: 5H,6H,7H-benzo[c]carbazole
• CAS No.: 5425-53-6
• Molecular Formula: C16H13N
• Molecular Weight: 219.286
• Hs Code.: 2933990090
• Mol file: 5425-53-6.mol

Synonyms:5,6-dihydro-benzo[c]carbazole;5,7-dihydro-6H-benzo[c]carbazole;5,6-dihydro-7H-benzocarbazole;6,7-dihydro-5H-benzocarbazole;6,7-Dihydro-5H-benzo[c]carbazol;

Chemical Property of 5H,6H,7H-benzo[c]carbazole

Chemical Property:

• Vapor Pressure: 5.31E-07mmHg at 25°C
• Boiling Point: 423.9oC at 760 mmHg
• Flash Point: 190.6oC
• PSA: 15.79000
• Density: 1.228g/cm3
• LogP: 3.93350

Purity/Quality:

98.5% ^*data from raw suppliers

6,7-DIHYDRO-5H-BENZO[C]CARBAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5H,6H,7H-benzo[c]carbazole

There total 2 articles about 5H,6H,7H-benzo[c]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

3-iodo-2-phenethyl-1H-indole → 2-(2-phenylethyl)-1H-indole (98055-06-2) + 5,6-dihydro-7H-benzocarbazole (5425-53-6)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 90h;

DOI:10.1016/S0040-4039(03)00094-7

Reference yield:

ethanol (64-17-5) + (E)-3-Ureido-but-2-enoic acid ethyl ester (5435-44-9,22243-66-9) + 3,4-dihydro-1H-naphthalen-2-one phenylhydrazone (83160-35-4) → 11H-benzo[a]carbazole (239-01-0) + 5,6-dihydro-7H-benzocarbazole (5425-53-6)

Guidance literature:

Reference yield: 96.0%

5,6-dihydro-7H-benzocarbazole (5425-53-6) → benzo[c]carbazole (205-25-4)

Guidance literature:

With chloranil; In xylene; for 2h; Inert atmosphere; Reflux;

upstream raw materials:

ethanol

(E)-3-Ureido-but-2-enoic acid ethyl ester

3,4-dihydro-1H-naphthalen-2-one phenylhydrazone

Downstream raw materials:

benzo[c]carbazole

7-phenyl-7H-benzo[c]carbazole

10-bromo-7-phenyl-7H-benzo[c]carbazole

C₂₈H₁₈ClN