1-Acetoxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime

Base Information

Chemical Name:1-Acetoxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime
CAS No.:145071-52-9
Molecular Formula:C₉H₁₄N₂O₃
Molecular Weight:198.222
Hs Code.:

Synonyms:BRN 5811985;1-Acetoxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime;(E)-1,2,5,6-Tetrahydro-1-(acetyloxy)-3-pyridinecarboxaldehyde 3-(O-methyloxime);3-Pyridinecarboxaldehyde, 1,2,5,6-tetrahydro-1-(acetyloxy)-, 3-(O-methyloxime), (E)-;145071-52-9;LS-130478

Suppliers and Price of 1-Acetoxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Acetoxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:321.2°Cat760mmHg
Flash Point:148.1°C
Density:1.09g/cm³
XLogP3:0.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:182.105527694
Heavy Atom Count:13
Complexity:246

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)N1CCC=C(C1)C=NOC
Isomeric SMILES:CC(=O)N1CCC=C(C1)/C=N/OC

Technology Process of 1-Acetoxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime

There total 2 articles about 1-Acetoxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 121750-98-9
1-hydroxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime

: 75-36-5
acetyl chloride

: 145071-52-9
1-acetoxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime

Guidance literature:: With triethylamine; In tetrahydrofuran; for 0.166667h; Ambient temperature;
DOI:10.1016/0223-5234(92)90186-5

Reference yield:

: 72989-57-2
pyridine-3-carboxaldehyde-O-methyloxime-N-oxide

: 145071-52-9
1-acetoxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 1 h / Ambient temperature

2: 79 percent / triethylamine / tetrahydrofuran / 0.17 h / Ambient temperature

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1016/0223-5234(92)90186-5