(4-METHOXY-2,3,6-TRIMETHYLBENZYL)-TRIPHENYLPHOSPHONIUM BROMIDE

Base Information

Chemical Name:(4-METHOXY-2,3,6-TRIMETHYLBENZYL)-TRIPHENYLPHOSPHONIUM BROMIDE
CAS No.:54486-05-4
Molecular Formula:C29H30OP.Br
Molecular Weight:505.42600
Hs Code.:
Mol file:54486-05-4.mol

Synonyms:Bromo(4-methoxy-2,3,6-trimethylbenzyl)triphenylphosphorane;

Suppliers and Price of (4-METHOXY-2,3,6-TRIMETHYLBENZYL)-TRIPHENYLPHOSPHONIUM BROMIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(4-Methoxy-2,3,6-trimethylbenzyl)-triphenylphosphoniumBromide
100mg
$ 140.00

Medical Isotopes, Inc.
(4-Methoxy-2,3,6-trimethylbenzyl)-triphenylphosphoniumBromide
0.5 g
$ 2000.00

American Custom Chemicals Corporation
(4-METHOXY-2,3,6-TRIMETHYLBENZYL)-TRIPHENYLPHOSPHONIUM BROMIDE 95.00%
1G
$ 1732.50

American Custom Chemicals Corporation
(4-METHOXY-2,3,6-TRIMETHYLBENZYL)-TRIPHENYLPHOSPHONIUM BROMIDE 95.00%
500MG
$ 739.20

Total 6 raw suppliers

Chemical Property of (4-METHOXY-2,3,6-TRIMETHYLBENZYL)-TRIPHENYLPHOSPHONIUM BROMIDE

Chemical Property:

PSA：22.82000
LogP:6.96010
Solubility.:Chloroform, Dichloromethane, Ethanol, Methanol

Purity/Quality:

98%Min ^*data from raw suppliers

(4-Methoxy-2,3,6-trimethylbenzyl)-triphenylphosphoniumBromide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4-METHOXY-2,3,6-TRIMETHYLBENZYL)-TRIPHENYLPHOSPHONIUM BROMIDE

There total 4 articles about (4-METHOXY-2,3,6-TRIMETHYLBENZYL)-TRIPHENYLPHOSPHONIUM BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 54344-93-3
(4-methoxy-2,3,6-trimethylphenyl)methanol

: 603-35-0
triphenylphosphine

: 54486-05-4
(4-Methoxy-2,3,6-trimethylbenzyl)triphenylphosphoniumbromid

Guidance literature:: With hydrogenchloride; In methanol; water; for 96h; Ambient temperature;
DOI:10.1002/jlac.198419841014

Reference yield:

: 20469-61-8
2,3,5-trimethylanisole

: 54486-05-4
(4-Methoxy-2,3,6-trimethylbenzyl)triphenylphosphoniumbromid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) POCl₃ / 1.) 0 deg C, 2 h, 2.) 70 deg, 24 h

2: 93 percent / LiAlH₄

3: 95 percent / 38 percent HCl / methanol; H₂O / 96 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; trichlorophosphate; In methanol; water;
DOI:10.1002/jlac.198419841014

Reference yield:

: 697-82-5
2,3,5-trimethylphenol

: 54486-05-4
(4-Methoxy-2,3,6-trimethylbenzyl)triphenylphosphoniumbromid

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / KOH / 0.5 h / Heating

2: 1.) POCl₃ / 1.) 0 deg C, 2 h, 2.) 70 deg, 24 h

3: 93 percent / LiAlH₄

4: 95 percent / 38 percent HCl / methanol; H₂O / 96 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; trichlorophosphate; In methanol; water;
DOI:10.1002/jlac.198419841014