1,1-Dichloro-2,2-diethoxyethene

Base Information

• Chemical Name: 1,1-Dichloro-2,2-diethoxyethene
• CAS No.: 54567-93-0
• Molecular Formula: C6H10Cl2O2
• Molecular Weight: 185.05
• DSSTox Substance ID: DTXSID40550039
• Nikkaji Number: J797.732H
• Wikidata: Q82429249

Synonyms:54567-93-0;1,1-Dichloro-2,2-diethoxyethene;DTXSID40550039

Chemical Property of 1,1-Dichloro-2,2-diethoxyethene

Chemical Property:

• XLogP3: 2.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 184.0057849
• Heavy Atom Count: 10
• Complexity: 111

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=C(Cl)Cl)OCC

Technology Process of 1,1-Dichloro-2,2-diethoxyethene

There total 1 articles about 1,1-Dichloro-2,2-diethoxyethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

1,1,1-trichloro-2,2-diethoxy-ethane (599-97-3) + sodium diethyl phosphite (2303-76-6,118080-94-7) → 1,1-dichloro-2,2-diethoxy-ethene (54567-93-0) + Diethyl phosphonate (762-04-9,123-22-8) + dichloro(diethoxyphosphinyl)acetaldehyde diethyl acetal (113827-81-9)

Guidance literature:

In benzene; for 2h; Heating;

Reference yield:

1,1-dichloro-2,2-diethoxy-ethene (54567-93-0) → ethyl 1,1-dichloroacetate (535-15-9)

Guidance literature:

With hydrogenchloride; water; In [D₃]acetonitrile;

DOI:10.1016/S0040-4020(01)88793-7

upstream raw materials:

1,1,1-trichloro-2,2-diethoxy-ethane

sodium diethyl phosphite

Downstream raw materials:

ethyl 1,1-dichloroacetate

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