6-CHLORO-2-HYDROXYQUINOLINE

Base Information

• Chemical Name: 6-CHLORO-2-HYDROXYQUINOLINE
• CAS No.: 1810-67-9
• Molecular Formula: C9H6 Br N O
• Molecular Weight: 179.606
• Hs Code.: 2933499090
• Mol file: 1810-67-9.mol

Synonyms:Carbostyril,6-bromo- (7CI,8CI); 6-Bromo-2(1H)-quinolinone; 6-Bromo-2(1H)-quinolone;6-Bromo-2-hydroxyquinoline; 6-Bromo-2-quinolinol; 6-Bromocarbostyril

Chemical Property of 6-CHLORO-2-HYDROXYQUINOLINE

Chemical Property:

• Melting Point: 265-269 °C(lit.)
• Boiling Point: 380.3°Cat760mmHg
• PKA: 10.76±0.70(Predicted)
• Flash Point: 183.8°C
• PSA: 32.86000
• Density: 1.339g/cm³
• LogP: 2.18150
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

6-Chloro-2-hydroxyquinoline 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-CHLORO-2-HYDROXYQUINOLINE

There total 23 articles about 6-CHLORO-2-HYDROXYQUINOLINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

6-chloroquinoline (612-57-7) → 6-chloroquinolin-2(1H)-oney (1810-67-9)

Guidance literature:

With water; chloroacetic acid ethyl ester; In ethyl acetate; for 0.5h; Microwave irradiation;

Reference yield: 88.0%

5-Chloro-2-<(2,2-dimethyl-1-oxopropyl)amino>-β-hydroxybenzenepropanoic Acid, 1,1-Dimethylethyl Ester (127472-36-0) → 6-chloroquinolin-2(1H)-oney (1810-67-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 4h; Heating;

DOI:10.1021/jo00302a049

Reference yield: 85.0%

6-chloroquinoline N-oxide (6563-10-6) → 6-chloroquinolin-2(1H)-oney (1810-67-9)

Guidance literature:

With 1,8-dimethoxy-10-phenyl-9-(o-tolyl)acridin-10-ium chloride; In dimethyl sulfoxide; at 20 ℃; for 8h; Irradiation; Green chemistry;

DOI:10.1039/d1gc01460a

upstream raw materials:

2,6-dichloroquinoline

6-chloroquinoline

6-chloroquinoline N-oxide

5-Chloro-2-<(2,2-dimethyl-1-oxopropyl)amino>-β-hydroxybenzenepropanoic Acid, 1,1-Dimethylethyl Ester

Downstream raw materials:

2,6-dichloroquinoline

5-chloroindole 2,3-dione

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