3,3,5,7-Tetramethyl-1-indanone

Base Information

Chemical Name:3,3,5,7-Tetramethyl-1-indanone
CAS No.:54789-23-0
Molecular Formula:C13H16O
Molecular Weight:188.26600
Hs Code.:2914399090
Mol file:54789-23-0.mol

Synonyms:3,3,5,7-Tetramethyl-indanon;3,3,5,7-tetramethyl-indan-1-one;1H-Inden-1-one, 2,3-dihydro-3,3,5,7-tetramethyl-;3,3,5,7-Tetramethyl-indan-1-on;3,3,5,7-Tetramethyl-1-indanon;3,3,5,7-tetramethyl-1-indanone;3,3,5,7-tetramethyl indane-1-one;2,3-dihydro-3,3,5,7-tetramethyl-1H-inden-1-one;1H-Inden-1-one,2,3-dihydro-3,3,5,7-tetramethyl;

Suppliers and Price of 3,3,5,7-Tetramethyl-1-indanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of 3,3,5,7-Tetramethyl-1-indanone

Chemical Property:

Melting Point:57.5-58 °C
Boiling Point:168-170 °C(Press: 35 Torr)
PSA：17.07000
Density:1.012±0.06 g/cm3(Predicted)
LogP:3.16740

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,3,5,7-Tetramethyl-1-indanone

There total 9 articles about 3,3,5,7-Tetramethyl-1-indanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 541-47-9
3-Methylbutenoic acid

: 108-38-3,104809-90-7
m-xylene

: 54789-23-0
3,3,5,7-tetramethyl-1-indanone

: 55255-42-0
2,3-dihydro-3,3,4,6-tetramethyl-1H-inden-1-one

Guidance literature:: With niobium pentachloride; In dichloromethane; for 0.833333h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2015.06.061

Reference yield: 56.0%

: 201230-82-2
carbon monoxide

: C₁₃H₁₇F₃O₃S

: 54789-23-0
3,3,5,7-tetramethyl-1-indanone

Guidance literature:: With palladium(II) trifluoroacetate; 4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride; cesium pivalate; In ethylbenzene; at 140 ℃; for 24h; under 760.051 Torr;
DOI:10.1021/acscatal.9b03426

Reference yield:

: 541-47-9
3-Methylbutenoic acid

: 54789-23-0
3,3,5,7-tetramethyl-1-indanone

Guidance literature:: Multi-step reaction with 2 steps

1: aluminium chloride

2: concentrated sulfuric acid

With aluminium trichloride; sulfuric acid;
DOI:10.1021/ja01242a017 DOI:10.2747/1060-586X.18.3.183