2-(1,3-dithian-2-yl)-4-methoxyphenol

Base Information

Chemical Name:2-(1,3-dithian-2-yl)-4-methoxyphenol
CAS No.:54810-45-6
Molecular Formula:C₁₁H₁₄O₂S₂
Molecular Weight:242.363
Hs Code.:
Mol file:54810-45-6.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(1,3-dithian-2-yl)-4-methoxyphenol

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

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Technology Process of 2-(1,3-dithian-2-yl)-4-methoxyphenol

There total 1 articles about 2-(1,3-dithian-2-yl)-4-methoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 109-80-8
1.3-propanedithiol

: 672-13-9
2-hydroxy-5-methoxybenzaldehyde

: 54810-45-6
2-[1,3]Dithian-2-yl-4-methoxy-phenol

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 2h; Molecular sieve;
DOI:10.1002/adsc.201200510

Reference yield:

: 54810-45-6
2-[1,3]Dithian-2-yl-4-methoxy-phenol

: 1416161-46-0
C₂₀H₂₂O₃Si

: 1416161-47-1
C₂₀H₂₂O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran / 2 h / -41 °C

1.2: 2 h

2.1: N-Bromosuccinimide; triethylamine / acetone; water / 0.33 h / -23 °C

3.1: potassium iodide; potassium carbonate / acetone / 20 °C

4.1: dichloromethane / 20 °C / Photolysis; Schlenk technique; Acidic conditions

With N-Bromosuccinimide; n-butyllithium; potassium carbonate; triethylamine; potassium iodide; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1002/adsc.201200510