Benzeneethanol, 2-bromo-4-methoxy-5-(phenylmethoxy)-

Base Information

Chemical Name:Benzeneethanol, 2-bromo-4-methoxy-5-(phenylmethoxy)-
CAS No.:55323-56-3
Molecular Formula:C16H17BrO3
Molecular Weight:337.213
Hs Code.:

Synonyms:

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Chemical Property of Benzeneethanol, 2-bromo-4-methoxy-5-(phenylmethoxy)-

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Technology Process of Benzeneethanol, 2-bromo-4-methoxy-5-(phenylmethoxy)-

There total 7 articles about Benzeneethanol, 2-bromo-4-methoxy-5-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 697803-44-4
1-Benzyloxy-4-bromo-2-methoxy-5-vinyl-benzene

: 55323-56-3
2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethanol

Guidance literature:: 1-Benzyloxy-4-bromo-2-methoxy-5-vinyl-benzene; With sodium tetrahydroborate; tin(IV) chloride; In tetrahydrofuran; for 7h;

With dihydrogen peroxide; In tetrahydrofuran;
DOI:10.1021/jo030287t

Reference yield:

: 621-59-0
isovanillin

: 55323-56-3
2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: Br₂ / acetic acid / 2 h / 25 °C

2.1: K₂CO₃ / ethanol / 2 h / 75 °C

3.1: 89 percent / CrCl₃; LAH / tetrahydrofuran / 6 h / 65 °C

4.1: 90 percent / LAH / tetrahydrofuran / 8 h / Heating

5.1: SnCl₄; NaBH₄ / tetrahydrofuran / 7 h

5.2: 92 percent / hydrogen peroxide / tetrahydrofuran

With chromium chloride; sodium tetrahydroborate; lithium aluminium tetrahydride; bromine; tin(IV) chloride; potassium carbonate; In tetrahydrofuran; ethanol; acetic acid;
DOI:10.1021/jo030287t

Reference yield:

: 2973-59-3
2-bromoisovanillin

: 55323-56-3
2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: K₂CO₃ / ethanol / 2 h / 75 °C

2.1: 89 percent / CrCl₃; LAH / tetrahydrofuran / 6 h / 65 °C

3.1: 90 percent / LAH / tetrahydrofuran / 8 h / Heating

4.1: SnCl₄; NaBH₄ / tetrahydrofuran / 7 h

4.2: 92 percent / hydrogen peroxide / tetrahydrofuran

With chromium chloride; sodium tetrahydroborate; lithium aluminium tetrahydride; tin(IV) chloride; potassium carbonate; In tetrahydrofuran; ethanol;
DOI:10.1021/jo030287t