Methyl 2-(butylamino)benzoate

Base Information

Chemical Name:Methyl 2-(butylamino)benzoate
CAS No.:55369-70-5
Molecular Formula:C12H17NO2
Molecular Weight:207.272
Hs Code.:
DSSTox Substance ID:DTXSID201263120
Nikkaji Number:J169.118J

Synonyms:methyl 2-(butylamino)benzoate;55369-70-5;methyl2-(butylamino)benzoate;DTXSID201263120;AKOS002665769;o-(Butylamino)benzoic acid methyl ester;CS-0261521;Benzoic acid, 2-(butylamino)-, methyl ester;EN300-78821;Z54131031

Suppliers and Price of Methyl 2-(butylamino)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Methyl 2-(butylamino)benzoate

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:207.125928785
Heavy Atom Count:15
Complexity:194

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCNC1=CC=CC=C1C(=O)OC

Technology Process of Methyl 2-(butylamino)benzoate

There total 4 articles about Methyl 2-(butylamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: methyl 2-((N-butyl-4-methylphenyl)sulfonamido)benzoate

: 55369-70-5
methyl 2-(butylamino)benzoate

Guidance literature:: With trifluorormethanesulfonic acid; In 1,2-dichloro-ethane; at 25 - 90 ℃; for 4h; Inert atmosphere;
DOI:10.1021/acs.joc.7b02507

Reference yield:

: 134-20-3
2-carbomethoxyaniline

: 107-92-6
butyric acid

: 55369-70-5
methyl 2-(butylamino)benzoate

Guidance literature:: With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; phenylsilane; 1,2-bis-(diphenylphosphino)ethane; In dibutyl ether; at 20 ℃; for 18h; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja5093612

Reference yield:

: 50998-74-8
methyl N-tosylanthranilate

: 55369-70-5
methyl 2-(butylamino)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 46 h / 80 °C

2: trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 4 h / 25 - 90 °C / Inert atmosphere

With trifluorormethanesulfonic acid; sodium hydride; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/acs.joc.7b02507