2,2-Dimethyl-4,5-diphenyl-2H-1,3,2-dioxasilole

Base Information

Chemical Name:2,2-Dimethyl-4,5-diphenyl-2H-1,3,2-dioxasilole
CAS No.:55629-19-1
Molecular Formula:C₁₆H₁₆O₂Si
Molecular Weight:268.387
Hs Code.:
DSSTox Substance ID:DTXSID10579459
Wikidata:Q82469983

Synonyms:55629-19-1;2,2-Dimethyl-4,5-diphenyl-2H-1,3,2-dioxasilole;DTXSID10579459

Suppliers and Price of 2,2-Dimethyl-4,5-diphenyl-2H-1,3,2-dioxasilole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-Dimethyl-4,5-diphenyl-2H-1,3,2-dioxasilole

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:268.091956283
Heavy Atom Count:19
Complexity:318

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si]1(OC(=C(O1)C2=CC=CC=C2)C3=CC=CC=C3)C

Technology Process of 2,2-Dimethyl-4,5-diphenyl-2H-1,3,2-dioxasilole

There total 4 articles about 2,2-Dimethyl-4,5-diphenyl-2H-1,3,2-dioxasilole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119-53-9,579-44-2
2-hydroxy-2-phenylacetophenone

: 55629-19-1
2,2-dimethyl-4,5-diphenyl-[1,3,2]dioxasilole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dibutyltin oxide / 1.) benzene, reflux, 1 h, 2.) toluene, room temperature, 1 h

2: 1.) dibutyltin oxide / 1.) toluene, reflux, 1 h, 2.) toluene, 0 deg C, 20 min ---> room temperature

With di(n-butyl)tin oxide;
DOI:10.1039/P19830000875

Reference yield:

: 21240-34-6
4,5-diphenyl-1,3-dioxol-2-one

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 55629-19-1
2,2-dimethyl-4,5-diphenyl-[1,3,2]dioxasilole

Guidance literature:: With di(n-butyl)tin oxide; Yield given. Multistep reaction; 1.) toluene, reflux, 1 h, 2.) toluene, 0 deg C, 20 min ---> room temperature;
DOI:10.1039/P19830000875

Reference yield:

: 119-53-9,579-44-2
2-hydroxy-2-phenylacetophenone

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 55629-19-1
2,2-dimethyl-4,5-diphenyl-[1,3,2]dioxasilole

Guidance literature:: With di(n-butyl)tin oxide; Yield given. Multistep reaction; 1.) benzene, reflux, 1 h, 2.) toluene, 0 deg C, 20 min ---> room temperature;
DOI:10.1039/P19830000875