Phenol, 3-(tributylstannyl)-

Base Information

Chemical Name:Phenol, 3-(tributylstannyl)-
CAS No.:557766-32-2
Molecular Formula:C₁₈H₃₂OSn
Molecular Weight:383.161
Hs Code.:

Synonyms:

Suppliers and Price of Phenol, 3-(tributylstannyl)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenol, 3-(tributylstannyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phenol, 3-(tributylstannyl)-

There total 1 articles about Phenol, 3-(tributylstannyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: (3-(tri-n-butylstannyl)phenoxy)(tert-butyl)dimethylsilane

: 557766-32-2
tributyl(3-hydroxyphenyl)tin

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; (Ar); addn. of tin compd. to a soln. of ammonium salt in THF, stirring at room temp. for 1 h; pouring into satd. aq. NH4Cl, extn. with ethyl acetate, washing org. phase with water, brine, drying (MgSO4), evapn., column chromy. (silica gel, hexane/ethyl acetate 20:1); elem. anal.;
DOI:10.1016/S0022-328X(02)02153-8

Reference yield: 84.0%

: 557766-32-2
tributyl(3-hydroxyphenyl)tin

: 79-22-1
methyl chloroformate

: 198202-09-4
tributyl(3-methoxycarbonyloxyphenyl)tin

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; (Ar); addn. of a soln. of tin compd. in THF to a suspn. of NaH in mineral oil at 0°C, stirring for 0.5 h at room temp., addn. of chloroformate, stirring overnight; pouring into satd. aq. NH4Cl, extn. with ethyl acetate, washing org. phase with water, brine, drying (MgSO4), evapn., column chromy. (silica gel, hexane/ethyl acetate 10:1); elem. anal.;
DOI:10.1016/S0022-328X(02)02153-8