2,6,11,15-Tetraazaoctadecanoic acid, 17-amino-6,11-bis[(1,1-dimethylethoxy)carbonyl]-18-[4-(1,1-dimethyleth oxy)phenyl]-16-oxo-, 1,1-dimethylethyl ester, (17S)-

Base Information

Chemical Name:2,6,11,15-Tetraazaoctadecanoic acid, 17-amino-6,11-bis[(1,1-dimethylethoxy)carbonyl]-18-[4-(1,1-dimethyleth oxy)phenyl]-16-oxo-, 1,1-dimethylethyl ester, (17S)-
CAS No.:557792-64-0
Molecular Formula:C38H67N5O8
Molecular Weight:721.979
Hs Code.:

2,6,11,15-Tetraazaoctadecanoic acid,
17-amino-6,11-bis[(1,1-dimethylethoxy)carbonyl]-18-[4-(1,1-dimethyleth
oxy)phenyl]-16-oxo-, 1,1-dimethylethyl ester, (17S)-

Synonyms:

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Chemical Property of 2,6,11,15-Tetraazaoctadecanoic acid, 17-amino-6,11-bis[(1,1-dimethylethoxy)carbonyl]-18-[4-(1,1-dimethyleth oxy)phenyl]-16-oxo-, 1,1-dimethylethyl ester, (17S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2,6,11,15-Tetraazaoctadecanoic acid, 17-amino-6,11-bis[(1,1-dimethylethoxy)carbonyl]-18-[4-(1,1-dimethyleth oxy)phenyl]-16-oxo-, 1,1-dimethylethyl ester, (17S)-

There total 3 articles about 2,6,11,15-Tetraazaoctadecanoic acid, 17-amino-6,11-bis[(1,1-dimethylethoxy)carbonyl]-18-[4-(1,1-dimethyleth oxy)phenyl]-16-oxo-, 1,1-dimethylethyl ester, (17S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (3-tert-butoxycarbonylamino-propyl)-[4-(tert-butoxycarbonyl-{3-[3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionylamino]-propyl}-amino)-butyl]-carbamic acid tert-butyl ester

: 557792-64-0
[4-({3-[2-amino-3-(4-tert-butoxy-phenyl)-propionylamino]-propyl}-tert-butoxycarbonyl-amino)-butyl]-(3-tert-butoxycarbonylamino-propyl)-carbamic acid tert-butyl ester

Guidance literature:: With Octanethiol; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/S0223-5234(02)00003-X

Reference yield:

: 114459-62-0
tri-Boc-spermine

: 557792-64-0
[4-({3-[2-amino-3-(4-tert-butoxy-phenyl)-propionylamino]-propyl}-tert-butoxycarbonyl-amino)-butyl]-(3-tert-butoxycarbonylamino-propyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 20 h / 20 °C

2: 2.60 g / octanethiol; DBU / tetrahydrofuran / 24 h / 20 °C

With Octanethiol; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0223-5234(02)00003-X

Reference yield:

: 86060-93-7
Fmoc-Tyr(tBu)-OPfp

: 557792-64-0
[4-({3-[2-amino-3-(4-tert-butoxy-phenyl)-propionylamino]-propyl}-tert-butoxycarbonyl-amino)-butyl]-(3-tert-butoxycarbonylamino-propyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 20 h / 20 °C

2: 2.60 g / octanethiol; DBU / tetrahydrofuran / 24 h / 20 °C

With Octanethiol; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0223-5234(02)00003-X