N-hexyl-2-iodoacetamide

Base Information

• Chemical Name: N-hexyl-2-iodoacetamide
• CAS No.: 5345-63-1
• Molecular Formula: C8H16INO
• Molecular Weight: 269.1232
• Mol file: 5345-63-1.mol

Synonyms:

Chemical Property of N-hexyl-2-iodoacetamide

Chemical Property:

• Vapor Pressure: 0.000137mmHg at 25°C
• Boiling Point: 333.4°C at 760 mmHg
• Flash Point: 155.4°C
• Density: 1.451g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-hexyl-2-iodoacetamide

There total 2 articles about N-hexyl-2-iodoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N-2-chloroethanoyl-hexylamine (5326-81-8) → N-(iodoacetyl)-n-hexylamine (5345-63-1)

Guidance literature:

With sodium iodide; In acetone; at 20 ℃; for 24h;

DOI:10.1139/cjc-2012-0358

Reference yield:

hexan-1-amine (111-26-2) → N-(iodoacetyl)-n-hexylamine (5345-63-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium carbonate / N,N-dimethyl-formamide / 24 h / 0 - 20 °C

2: sodium iodide / acetone / 24 h / 20 °C

With sodium carbonate; sodium iodide; In N,N-dimethyl-formamide; acetone;

DOI:10.1139/cjc-2012-0358

upstream raw materials:

hexan-1-amine

N-2-chloroethanoyl-hexylamine

Refernces