Phenetole, beta,beta'-thiodi-

Base Information

• Chemical Name: Phenetole, beta,beta'-thiodi-
• CAS No.: 13755-14-1
• Molecular Formula: C₁₆H₁₈O₂S
• Molecular Weight: 274.384
• NSC Number: 42909
• DSSTox Substance ID: DTXSID00160234
• Wikidata: Q83028598
• Mol file: 13755-14-1.mol

Synonyms:Phenetole, beta,beta'-thiodi-;13755-14-1;beta,beta'-Thiodiphenetole;Bis(2-phenoxyethyl)sulfide;Thiodiethanol diphenyl ether;Bis(beta-phenoxy-ethyl)sulfide;2-(2-phenoxyethylsulfanyl)ethoxybenzene;BRN 1978936;Benzene, 1,1'-(thiobis(2,1-ethanediyloxy))bis-;NSC42909;bis(2-phenoxyethyl) sulfide;Bis(2-phenoxy-ethyl)sulfide;4-06-00-00581 (Beilstein Handbook Reference);SCHEMBL8671561;DTXSID00160234;NSC 42909;NSC-42909;AKOS016996754

Chemical Property of Phenetole, beta,beta'-thiodi-

Chemical Property:

• Boiling Point: 422.8°Cat760mmHg
• Flash Point: 209.5°C
• Density: 1.118g/cm³
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 8
• Exact Mass: 274.10275099
• Heavy Atom Count: 19
• Complexity: 189

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)OCCSCCOC2=CC=CC=C2

Technology Process of Phenetole, beta,beta'-thiodi-

There total 6 articles about Phenetole, beta,beta'-thiodi- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-thiobis-ethanol (111-48-8) + phenol (108-95-2,27073-41-2) → bis(2-phenoxyethyl)sulfide (13755-14-1)

Guidance literature:

With toluene-4-sulfonic acid; xylene; unter Entfernen des entstehenden Wassers;

DOI:10.1021/ja01136a031

Reference yield:

bis(2-bromoethyl)sulfide (7617-64-3) + phenol (108-95-2,27073-41-2) → bis(2-phenoxyethyl)sulfide (13755-14-1)

Guidance literature:

With potassium carbonate; In acetone; for 3h; Reflux;

DOI:10.1177/1469066719886424

Reference yield:

bis (2-chloroethyl) sulphide (505-60-2) + sodium phenoxide (139-02-6) → bis(2-phenoxyethyl)sulfide (13755-14-1)

Guidance literature:

upstream raw materials:

bis (2-chloroethyl) sulphide

sodium phenoxide

vinyl phenyl ether

2,2'-thiobis-ethanol