D-Tyrosine, N-[(phenylmethoxy)carbonyl]-, ethyl ester

Base Information

Chemical Name:D-Tyrosine, N-[(phenylmethoxy)carbonyl]-, ethyl ester
CAS No.:562813-10-9
Molecular Formula:C₁₉H₂₁NO₅
Molecular Weight:343.379
Hs Code.:

Synonyms:

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Chemical Property of D-Tyrosine, N-[(phenylmethoxy)carbonyl]-, ethyl ester

Chemical Property:

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Technology Process of D-Tyrosine, N-[(phenylmethoxy)carbonyl]-, ethyl ester

There total 2 articles about D-Tyrosine, N-[(phenylmethoxy)carbonyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23234-44-8
D-tyrosine ethyl ester

: 501-53-1,94274-21-2
benzyl chloroformate

: 562813-10-9
(R)-2-Benzyloxycarbonylamino-3-(4-hydroxy-phenyl)-propionic acid ethyl ester

Guidance literature:: With potassium carbonate; In water; ethyl acetate; at 3 - 8 ℃; for 0.5h;
DOI:10.1080/00397919808007167

Reference yield:

: 556-02-5,18875-48-4,25619-78-7,30704-25-7
tyrosine

: 562813-10-9
(R)-2-Benzyloxycarbonylamino-3-(4-hydroxy-phenyl)-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / Ambient temperature

2: K₂CO₃ / ethyl acetate; H₂O / 0.5 h / 3 - 8 °C

With thionyl chloride; potassium carbonate; In water; ethyl acetate;
DOI:10.1080/00397919808007167

Reference yield:

: 562813-10-9
(R)-2-Benzyloxycarbonylamino-3-(4-hydroxy-phenyl)-propionic acid ethyl ester

: 50505-81-2,52740-56-4
(+)-4-Methoxyamphetamine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / dimethylsulfoxide / 16 h / Ambient temperature

2: 65 percent / NaBH₄ / ethanol / 7 h / Ambient temperature

3: 86 percent / aq. NaOH, n-Bu₄NHSO₄ / benzene; H₂O / 0.5 h / 15 - 20 °C

4: 85 percent / NaI, Zn / tetrahydrofuran; H₂O / 2 h / Heating

5: 80.3 percent / H₂, aq. HCl / Pd-C / tetrahydrofuran / 3 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; sodium iodide; zinc; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide; benzene;
DOI:10.1080/00397919808007167