N-Acetyl-DL-valine ethyl ester

Base Information

Chemical Name:N-Acetyl-DL-valine ethyl ester
CAS No.:56430-36-5
Molecular Formula:C9H17NO3
Molecular Weight:187.239
Hs Code.:
Mol file:56430-36-5.mol

Synonyms:ethyl N-acetyl-valinate;N-Acetyl-DL-valin-aethylester;N-Acetyl-D,L-valin-ethylester;N-Acetyl-valin-aethylester;N-acetyl-DL-valine ethyl ester;

Suppliers and Price of N-Acetyl-DL-valine ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-Acetyl-DL-valine ethyl ester

Chemical Property:

PSA：55.40000
LogP:1.10110

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Acetyl-DL-valine ethyl ester

There total 6 articles about N-Acetyl-DL-valine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 78-39-7
Triethyl orthoacetate

: 516-06-3,25609-85-2,7004-03-7,921-10-8
D,L-valine

: 56430-36-5
(RS)-N-acetyl valine ethyl ester

Guidance literature:: In toluene; at 110 ℃; for 24h;
DOI:10.1016/j.tetlet.2010.10.081

Reference yield:

: 77920-68-4
2-acetylamino-3-methyl-crotonic acid ethyl ester

: 56430-36-5
(RS)-N-acetyl valine ethyl ester

Guidance literature:: With hydrogen; {(1,5-cyclooctadiene)Rh(1,2-bis((2R,5R)-2,5-dimethylphospholano)benzene)}triflate; In hexane; at 20 ℃; for 16h; under 413.729 Torr;
DOI:10.1039/b003354p

Reference yield:

: 4070-48-8
L-valine methyl ester

: 56430-36-5
(RS)-N-acetyl valine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaOCH₃ / Brenner esterification

2: pyridine

With pyridine; sodium methylate;
DOI:10.1016/S0040-4020(01)90011-0