Benzaldehyde, 4-iodo-3,5-dimethoxy-

Base Information

• Chemical Name: Benzaldehyde, 4-iodo-3,5-dimethoxy-
• CAS No.: 56518-59-3
• Molecular Formula: C9H9IO3
• Molecular Weight: 292.073
• Mol file: 56518-59-3.mol

Synonyms:4-iodo-3,5-dimethoxy-benzaldehyde;4-iodo-3,5-dimethoxybenzaldehyde;4-Iod-3,5-dimethoxy-benzaldehyd;

Chemical Property of Benzaldehyde, 4-iodo-3,5-dimethoxy-

Chemical Property:

• Melting Point: 127 - 128 °C
• Boiling Point: 366.2±42.0 °C(Predicted)
• PSA: 35.53000
• Density: 1.706±0.06 g/cm3(Predicted)
• LogP: 2.12090

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzaldehyde, 4-iodo-3,5-dimethoxy-

There total 1 articles about Benzaldehyde, 4-iodo-3,5-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3,5-dimethoxy-4-iodobenzaldehyde (56518-59-3)

Guidance literature:

4-Iod-3,5-dimethoxybenzoesaeuremethylester,THF 1. Diisobutyl-AlH,Hexan 2. MnO2,CH2Cl2;

DOI:10.1002/hlca.19770600854

Reference yield: 100.0%

diethoxyphosphoryl-acetic acid ethyl ester (867-13-0) + 3,5-dimethoxy-4-iodobenzaldehyde (56518-59-3) → (E)-3-(4-iodo-3,5-dimethoxyphenyl)-acrylic acid ethyl ester (912675-56-0)

Guidance literature:

diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In benzene; at 0 ℃; for 0.25h;

3,5-dimethoxy-4-iodobenzaldehyde; In benzene; at 0 - 20 ℃; for 1.5h;

DOI:10.1021/jo0611364

Reference yield: 99.0%

3,5-dimethoxy-4-iodobenzaldehyde (56518-59-3) + ethylene glycol (107-21-1) → 2-(4-iodo-3,5-dimethoxyphenyl)-(1,3)-dioxolane (403706-11-6)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 20h; Heating;

DOI:10.1021/jo0611364

Downstream raw materials:

2-(4-iodo-3,5-dimethoxy-benzyl)-3-morpholin-4-yl-acrylonitrile

2-(4-iodo-3,5-dimethoxyphenyl)-(1,3)-dioxolane

(E)-3-(4-iodo-3,5-dimethoxyphenyl)-acrylic acid ethyl ester

(E)-3-(4-iodo-3,5-dimethoxyphenyl)prop-2-en-1-ol