N-[(Benzyloxy)carbonyl]-L-valyl-N-methylglycine

Base Information

Chemical Name:N-[(Benzyloxy)carbonyl]-L-valyl-N-methylglycine
CAS No.:56609-93-9
Molecular Formula:C16H22N2O5
Molecular Weight:322.361
Hs Code.:
DSSTox Substance ID:DTXSID30576460
Wikidata:Q82466175

Synonyms:56609-93-9;N-[(Benzyloxy)carbonyl]-L-valyl-N-methylglycine;SCHEMBL7378215;benzyloxycarbonyl-l-valylsarcosine;DTXSID30576460

Suppliers and Price of N-[(Benzyloxy)carbonyl]-L-valyl-N-methylglycine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of N-[(Benzyloxy)carbonyl]-L-valyl-N-methylglycine

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:322.15287181
Heavy Atom Count:23
Complexity:419

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C(C(=O)N(C)CC(=O)O)NC(=O)OCC1=CC=CC=C1
Isomeric SMILES:CC(C)[C@@H](C(=O)N(C)CC(=O)O)NC(=O)OCC1=CC=CC=C1

Technology Process of N-[(Benzyloxy)carbonyl]-L-valyl-N-methylglycine

There total 3 articles about N-[(Benzyloxy)carbonyl]-L-valyl-N-methylglycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 138228-89-4
methyl N^2.1-<(benzyloxy)carbonyl>-L-valylsarcosinate

: 56609-93-9
N^2.1-<(benzyloxy)carbonyl>-L-valylsarcosine

Guidance literature:: With sodium hydroxide; In methanol; water; at 40 ℃; pH 11;
DOI:10.1002/hlca.19910740702

Reference yield:

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 56609-93-9
N^2.1-<(benzyloxy)carbonyl>-L-valylsarcosine

Guidance literature:: Multi-step reaction with 2 steps

1: 1) (i-Pr)2NEt, BOP-Cl / CH₂Cl₂, 1) <*>-15 deg C, 2 h 2) to r.t., 12 h

2: 96 percent / 1M NaOH / methanol; H₂O / 40 °C / pH 11

With sodium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In methanol; water;
DOI:10.1002/hlca.19910740702