Azidosulfuric acid, phenyl ester

Base Information

Chemical Name:Azidosulfuric acid, phenyl ester
CAS No.:57060-38-5
Molecular Formula:C6H5N3O3S
Molecular Weight:199.19
Hs Code.:

Synonyms:

Suppliers and Price of Azidosulfuric acid, phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Azidosulfuric acid, phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Azidosulfuric acid, phenyl ester

There total 2 articles about Azidosulfuric acid, phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 16475-29-9
phenylchlorosulfate

: 57060-38-5
phenoxysulfonyl azide

Guidance literature:: With tetrabutylammoniun azide; In benzene; at 20 ℃; for 0.166667h;

Reference yield:

: 108-95-2,27073-41-2
phenol

: 57060-38-5
phenoxysulfonyl azide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 0 °C / Inert atmosphere; Schlenk technique

1.2: 5 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: sodium azide / acetonitrile / 16 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With pyridine; sodium azide; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2015.01.186

Reference yield: 82.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 57060-38-5
phenoxysulfonyl azide

: phenyl 2‐phenylaziridine‐1-sulfonate

Guidance literature:: With cobalt(II) 5,10,15,20-tetraphenylporphyrin; In chlorobenzene; at 20 ℃; for 20h; Inert atmosphere; Schlenk technique; Molecular sieve;
DOI:10.1016/j.tetlet.2015.01.186