4,5-Isoxazoledicarboxylic acid, 4,5-dihydro-3-phenyl-, diethyl ester, trans-

Base Information

Chemical Name:4,5-Isoxazoledicarboxylic acid, 4,5-dihydro-3-phenyl-, diethyl ester, trans-
CAS No.:57065-93-7
Molecular Formula:C₁₅H₁₇NO₅
Molecular Weight:291.304
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,5-Isoxazoledicarboxylic acid, 4,5-dihydro-3-phenyl-, diethyl ester, trans-

Chemical Property:

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Technology Process of 4,5-Isoxazoledicarboxylic acid, 4,5-dihydro-3-phenyl-, diethyl ester, trans-

There total 8 articles about 4,5-Isoxazoledicarboxylic acid, 4,5-dihydro-3-phenyl-, diethyl ester, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 5585-14-8
3,4-diphenyl-furazan 2-oxide

: 623-91-6
diethyl Fumarate

: 57065-93-7,57065-94-8,91154-16-4
(4RS,5RS)-3-phenyl-4,5-dihydro-isoxazole-4,5-dicarboxylic acid diethyl ester

Guidance literature:: 3,4-diphenyl-furazan 2-oxide; Flash vacuum pyrolysis;

diethyl Fumarate; In toluene; Inert atmosphere;
DOI:10.3998/ark.5550190.0011.a04

Reference yield:

: 932-90-1
Benzaldoxime

: 623-91-6
diethyl Fumarate

: 57065-93-7,57065-94-8,91154-16-4
(4RS,5RS)-3-phenyl-4,5-dihydro-isoxazole-4,5-dicarboxylic acid diethyl ester

: 57065-93-7,57065-94-8,91154-16-4
(4SR,5RS)-3-phenyl-4,5-dihydro-isoxazole-4,5-dicarboxylic acid diethyl ester

Guidance literature:: With 2,6-dimethylpyridine; tert-butylhypochlorite; sodium iodide; In 1,4-dioxane; at 20 ℃; for 24h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol2010616

Reference yield:

: 932-90-1
Benzaldoxime

: 623-91-6
diethyl Fumarate

: 57065-93-7,57065-94-8,91154-16-4
(4RS,5RS)-3-phenyl-4,5-dihydro-isoxazole-4,5-dicarboxylic acid diethyl ester

: 57065-93-7,57065-94-8,91154-16-4
(4SR,5RS)-3-phenyl-4,5-dihydro-isoxazole-4,5-dicarboxylic acid diethyl ester

Guidance literature:: With 2,6-dimethylpyridine; tert-butylhypochlorite; sodium iodide; In 1,4-dioxane; at 20 ℃; for 24h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol2010616