[3-(Diphenylphosphanyl)propyl](methyl)phenylphosphane

Base Information

Chemical Name:[3-(Diphenylphosphanyl)propyl](methyl)phenylphosphane
CAS No.:57137-57-2
Molecular Formula:C22H24P2
Molecular Weight:350.38
Hs Code.:
DSSTox Substance ID:DTXSID80512757

Synonyms:57137-57-2;[3-(Diphenylphosphanyl)propyl](methyl)phenylphosphane;DTXSID80512757

Suppliers and Price of [3-(Diphenylphosphanyl)propyl](methyl)phenylphosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [3-(Diphenylphosphanyl)propyl](methyl)phenylphosphane

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:7
Exact Mass:350.13532476
Heavy Atom Count:24
Complexity:307

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CP(CCCP(C1=CC=CC=C1)C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of [3-(Diphenylphosphanyl)propyl](methyl)phenylphosphane

There total 3 articles about [3-(Diphenylphosphanyl)propyl](methyl)phenylphosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 57322-05-1
Diphenyl<3-(phenylphosphino)propyl>phosphin

: 74-88-4
methyl iodide

: 57137-57-2
(C₆H₅)2P(CH₂)3P(CH₃)(C₆H₅)

Guidance literature:: With n-butyllithium; In tetrahydrofuran; -78 deg C, 40 min, RT, 30 min;
DOI:10.1016/0022-328X(86)80279-0

Reference yield:

: 6737-42-4
1,3-bis-(diphenylphosphino)propane

: 57137-57-2
(C₆H₅)2P(CH₂)3P(CH₃)(C₆H₅)

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / naphthalene, sodium / tetrahydrofuran / 48 h / 0 - 22 °C

2: 92 percent / n-BuLi / tetrahydrofuran / -78 deg C, 40 min, RT, 30 min

With n-butyllithium; naphthalene; sodium; In tetrahydrofuran;
DOI:10.1016/0022-328X(86)80279-0