2-Ethyl-5,5-dimethyl-1,3,2-dioxaborinane

Base Information

Chemical Name:2-Ethyl-5,5-dimethyl-1,3,2-dioxaborinane
CAS No.:57186-59-1
Molecular Formula:C7H15BO2
Molecular Weight:142.00400
Hs Code.:
Mol file:57186-59-1.mol

Synonyms:2-Ethyl-5,5-dimethyl-1,3,2-dioxaboracyclohexan;1,3,2-Dioxaborinane,2-ethyl-5,5-dimethyl;

Suppliers and Price of 2-Ethyl-5,5-dimethyl-1,3,2-dioxaborinane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 2-Ethyl-5,5-dimethyl-1,3,2-dioxaborinane

Chemical Property:

Boiling Point:149.6±9.0 °C(Predicted)
PSA：18.46000
Density:0.88±0.1 g/cm3(Predicted)
LogP:1.56750

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Ethyl-5,5-dimethyl-1,3,2-dioxaborinane

There total 2 articles about 2-Ethyl-5,5-dimethyl-1,3,2-dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 4433-63-0
Ethyl boronic acid

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 57186-59-1
2-ethyl-5,5-dimethyl-1,3,2-dioxaborinane

Guidance literature:: In diethyl ether; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja409100y

Reference yield:

: 55848-38-9
diethylborinic acid 2,2-dimethyl-propane-1,3-diyl ester

: 57186-59-1
2-ethyl-5,5-dimethyl-1,3,2-dioxaborinane

Guidance literature:: With Diethylborane; Ambient temperature;

Reference yield: 84.0%

: 57186-59-1
2-ethyl-5,5-dimethyl-1,3,2-dioxaborinane

: (R)-(+)-1-(4-methoxyphenyl)ethyl N,N-diisopropylcarbamate

: (R)-2-(2-(4-methoxyphenyl)butan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane

Guidance literature:: (R)-(+)-1-(4-methoxyphenyl)ethyl N,N-diisopropylcarbamate; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether; at -78 ℃; for 0.166667h;

2-ethyl-5,5-dimethyl-1,3,2-dioxaborinane; In diethyl ether; at -78 - 20 ℃; for 17h;
DOI:10.1021/ja509029h