(4-AMino-phenyl)-cyclopropylMethanone

Base Information

• Chemical Name: (4-AMino-phenyl)-cyclopropylMethanone
• CAS No.: 57189-90-9
• Molecular Formula: C10H11NO
• Molecular Weight: 161.203
• Hs Code.: 2922399090
• Mol file: 57189-90-9.mol

Synonyms:p-Amino-phenyl-cyclopropyl-keton;(4-amino-phenyl)-cyclopropylmethanone;4-aminophenyl cyclopropyl ketone;

Chemical Property of (4-AMino-phenyl)-cyclopropylMethanone

Chemical Property:

• Boiling Point: 341.2±15.0 °C(Predicted)
• PKA: 2.21±0.10(Predicted)
• PSA: 43.09000
• Density: 1.216±0.06 g/cm3(Predicted)
• LogP: 2.44270

Purity/Quality:

97% ^*data from raw suppliers

4-cyclopropanecarbonylaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-AMino-phenyl)-cyclopropylMethanone

There total 10 articles about (4-AMino-phenyl)-cyclopropylMethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

cyclopropyl(4-nitrophenyl)methanone (93639-12-4) → (4-aminophenyl)(cyclopropyl)methanone (57189-90-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 0.75h; under 517.1 Torr;

DOI:10.1021/jm960441m

Reference yield: 90.0%

1-(4-acetylaminophenyl)-4-chloro-1-butanone (56924-11-9) → (4-aminophenyl)(cyclopropyl)methanone (57189-90-9)

Guidance literature:

With sodium hydroxide; In ethanol; for 2h; Heating;

DOI:10.1246/bcsj.70.681

Reference yield: 81.0%

4-aminophenylzinc iodide + cyclopropanecarboxylic acid chloride (4023-34-1) → (4-aminophenyl)(cyclopropyl)methanone (57189-90-9)

Guidance literature:

With copper(l) iodide; lithium chloride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.tetlet.2015.01.053

upstream raw materials:

cyclopropyl(4-nitrophenyl)methanone

1-(4-acetylaminophenyl)-4-chloro-1-butanone

Acetanilid

cyclopropyl phenyl ketone

Downstream raw materials:

cyclopropyl(4-nitrophenyl)methanone

haloperidol

spiperone

4-(4-chlorophenyl)-1-<4-(4-nitrophenyl)-4-oxobutyl>-4-piperidinol

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