2-methoxy-6-{[(3-methoxyphenyl)imino]methyl}phenol

Base Information

• Chemical Name: 2-methoxy-6-{[(3-methoxyphenyl)imino]methyl}phenol
• CAS No.: 57322-37-9
• Molecular Formula: C15H15NO3
• Molecular Weight: 257.289
• Mol file: 57322-37-9.mol

Synonyms:3-Methoxy-(2-hydroxy-3-methoxy-benzal)-anilin;2-Methoxy-6-{[(E)-3-methoxy-phenylimino]-methyl}-phenol;(2-Oxy-3-methoxy-benzal)-m-anisidin;

Chemical Property of 2-methoxy-6-{[(3-methoxyphenyl)imino]methyl}phenol

Chemical Property:

• Melting Point: 80 °C
• PSA: 51.05000
• LogP: 3.16000

Purity/Quality:

99% ^*data from raw suppliers

2-methoxy-6-{[(3-methoxyphenyl)imino]methyl}phenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-methoxy-6-{[(3-methoxyphenyl)imino]methyl}phenol

There total 2 articles about 2-methoxy-6-{[(3-methoxyphenyl)imino]methyl}phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-Anisidine (536-90-3,918666-97-4) + 3-methoxy-2-hydroxybenzaldehyde (148-53-8) → 2-Methoxy-6-[(3-methoxy-phenylimino)-methyl]-phenol (57322-37-9)

Guidance literature:

With ethanol;

Reference yield:

→ 2-Methoxy-6-[(3-methoxy-phenylimino)-methyl]-phenol (57322-37-9)

Guidance literature:

2-Hydroxy-3-methoxy-benzaldehyd, 3-Methoxy-anilin;

Reference yield: 79.0%

2-Methoxy-6-[(3-methoxy-phenylimino)-methyl]-phenol (57322-37-9) + methyltrioxorhenium(VII) (70197-13-6) → CH3ReO3(CH3OC6H3OCHNHC6H4OCH3)*CH3ReO3(CH3OC6H3OCHNHC6H4OCH3)

Guidance literature:

In diethyl ether; (Ar); dropwise addn. of a soln. of Re compd. in Et2O to a soln. of ligand in Et2O, stirring at room temp.; concn., recrystn. ppt. (CH2Cl2/n-hexane or Et2O/n-hexane); elem. anal.;

DOI:10.1016/j.jorganchem.2008.05.003

upstream raw materials:

m-Anisidine

3-methoxy-2-hydroxybenzaldehyde

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