2,2-Dichloronorbornane

Base Information

• Chemical Name: 2,2-Dichloronorbornane
• CAS No.: 19916-65-5
• Deprecated CAS: 67844-25-1
• Molecular Formula: C₇H₁₀Cl₂
• Molecular Weight: 165.062
• European Community (EC) Number: 243-425-9
• NSC Number: 176179
• DSSTox Substance ID: DTXSID70885104
• Nikkaji Number: J280.404B
• Mol file: 19916-65-5.mol

Synonyms:2,2-Dichloronorbornane;19916-65-5;2,2-Dichlorobicyclo[2.2.1]heptane;Norbornane, 2,2-dichloro-;Bicyclo[2.2.1]heptane, 2,2-dichloro-;EINECS 243-425-9;2,2-Dichlorobicyclo(2.2.1)heptane;NSC 176179;Bicyclo(2.2.1)heptane, 2,2-dichloro-;NSC176179;Norbornane,2-dichloro-;2,2-dichloronor-bornane;ClC1(Cl)CC2CCC1C2;C7H10Cl2;C7-H10-Cl2;DTXSID70885104;Bicyclo[2.2.1]heptane,2-dichloro-;NSC-176179;2,2-Dichlorobicyclo[2.2.1]heptane #

Chemical Property of 2,2-Dichloronorbornane

Chemical Property:

• Vapor Pressure: 0.312mmHg at 25°C
• Boiling Point: 208.2°Cat760mmHg
• Flash Point: 81.8°C
• PSA: 0.00000
• Density: 1.25g/cm³
• LogP: 2.98030
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 164.0159557
• Heavy Atom Count: 9
• Complexity: 131

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2CC1CC2(Cl)Cl

Technology Process of 2,2-Dichloronorbornane

There total 4 articles about 2,2-Dichloronorbornane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

Norbornan-2-on (497-38-1) → 2,2-dichlorobicyclo<2.2.1>heptane (19916-65-5,29583-37-7)

Guidance literature:

With phosphorus pentachloride; phosphorus trichloride; Ambient temperature;

DOI:10.1021/jo00085a012

Reference yield:

→ 2,2-dichlorobicyclo<2.2.1>heptane (19916-65-5,29583-37-7)

Guidance literature:

duch Reaktion v. Keten 7 m. PCl3/PCl5;

DOI:10.1021/ja00722a020

Reference yield:

2-norbornanone (497-38-1,2630-41-3,22270-13-9,29583-35-5) → 2,2-dichloronorbornane (19916-65-5,29583-37-7,67844-25-1)

Guidance literature:

With phosphorus pentachloride; phosphorus trichloride;

DOI:10.1021/jo01099a600

upstream raw materials:

Norbornan-2-on

2-norbornanone

(+/-)-endo-2-norborneol

Downstream raw materials:

1-chlorobicyclo[2.2.1]heptane

1,2-dichlorobicyclo<2.2.1>heptane

bicyclo<4.1.0>hep-2-en-1-ylmethanamine

p-bromobenzenesulphonamide bicyclo<4.1.0>hep-2-en-1-ylmethanamine